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r RECT JUL 2 4 2015 Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3 Job Number: C35685 Account: DECASM Dysert Environmental Project: Pactiv Packaging- 1110 Performance Drive Stockton CA 95206 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch C35719-5MS M48875.D 1 08/31/14 TN n/a n/a VM1482 C35719-5MSD M48876.D 1 08/31/14 TN n/a n/a VM1482 C35719-5 M48861.D 1 08/31/14 TN n/a n/a VM1482 m A The QC reported here applies to the following samples: Method: SW846 8260B =. C35685-1 C35719-5 Spike MS MS Spike MSD MSD Limits CAS No. Compound ug/kg Q ug/kg ug/kg % ug/kg ug/kg % RPD Rec/RPD 591-78-6 2-Hexanone ND 160 158 99 160 151 94 5 68-139/24 87-68-3 Hexachlorobutadiene ND 40 23.2 58* a 40 28.4 71*a 20 81-126/32 98-82-8 Isopropylbenzene ND 40 34.5 86 40 35.0 88 1 81-122/22 99-87-6 p-Isopropyltoluene ND 40 29.5 74* a 40 31.4 79*a 6 81-121/23 108-10-1 4-Methyl-2-pentanone ND 160 161 101 160 155 97 4 74-136/23 74-83-9 Methyl bromide ND 40 33.5 84 40 32.9 82 2 82-124/20 74-87-3 Methyl chloride ND 40 30.9 77 40 28.6 72 8 60-132/26 74-95-3 Methylene bromide ND 40 35.5 89 40 34.4 86 3 82-120/20 75-09-2 Methylene chloride ND 40 35.9 90 40 35.0 88 3 75-119/20 78-93-3 Methyl ethyl ketone NO 160 148 93 160 140 88 6 71-130/22 1634-04-4 Methyl Tert Butyl Ether NO 40 34.0 85 40 32.8 82 4 79-127/19 91-20-3 Naphthalene NO 40 25.2 63*a 40 24.6 62* a 2 78-125/23 103-65-1 n-Propylbenzene ND 40 31.3 78*a 40 32.3 81 3 79-124/22 100-42-5 Styrene NO 40 31.8 80*a 40 31.1 78* a 2 83-122/21 994-05-8 Tert-Amyl Methyl Ether NO 40 35.4 89 40 34.3 86 3 80-127/20 75-65-0 Tert Butyl Alcohol NO 200 211 106 200 200 100 5 65-144/23 630-20-6 1,1,1,2-Tetrachloroethane NO 40 35.1 88 40 34.8 87 1 82-123/21 71-55-6 1,1,1-Trichloroethane NO 40 36.8 92 40 36.0 90 2 79-129/21 79-34-5 1,1,2,2-Tetrachloroethane NO 40 33.6 84 40 32.4 81 4 77-126/20 79-00-5 1,1,2-Trichloroethane NO 40 35.3 88 40 34.1 85 3 79-123/20 87-61-6 1,2,3-Trichlorobenzene NO 40 21.6 54* a 40 22.3 56*a 3 81-122/26 96-18-4 1,2,3-Trichloropropane NO 40 35.4 89 40 34.3 86 3 79-122/24 120-82-1 1,2,4-Trichlorobenzene NO 40 20.4 51* a 40 21.1 53*a 3 81-121/26 95-63-6 1,2,4-Trimethylbenzene NO 40 29.8 75* a 40 30.1 75*a 1 82-121/24 108-67-8 1,3,5-Trimethylbenzene NO 40 31.8 80* a 40 32.5 81 2 81-123/23 127-18-4 Tetrachloroethylene ND 40 49.3 123 40 48.6 122 1 80-125/25 108-88-3 Toluene ND 40 36.8 92 40 36.3 91 1 80-117/21 79-01-6 Trichloroethylene ND 40 37.8 95 40 37.0 93 2 81-122/20 75-69-4 Trichlorofluoromethane NO 40 33.2 83 40 32.0 80 4 77-133/22 75-01-4 Vinyl chloride ND 40 33.0 83 40 32.5 81 2 71-133/23 1330-20-7 Xylene (total) ND 120 105 88 120 104 87 1 81-122/22 CAS No. Surrogate Recoveries MS MSD C35719-5 Limits 1868-53-7 Dibromofluoromethane 104% 102% 103% 70-130% * = Outside of Control Limits. 31 of 64 E ACCUTEST. C35685 I.....I--