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ACCUTEBT
<br /> I- AD ORATOR I C
<br /> SAMPLE DELIVERY GROUP CASE NARRATIVE
<br /> Client: Dysert Environmental Job No C35685
<br /> Site: Pactiv Packaging- 1110 Performance Drive Stockton CA 95206 Report Date 9/5/2014 7:39:15 PM
<br /> I Sample(s),0 Trip Blank(s)and 0 Field Blank(s)were collected on 08/26/2014 and were received at Accutest on 08/27/2014
<br /> properly preserved,at 3.3 Deg.C and intact,unless noted below. These Samples received an Accutest job number of C35685.A
<br /> listing of the Laboratory Sample 1D,Client Sample ID and dates of collection are presented in the Results Summary Section of this
<br /> report. *Note:Water matrices are performed on a volume basis.Due to the nature of the ink sample(adheres to measurement and
<br /> transfer vessels),we had to perform analyses on a weight basis and the only way to do that in our LIMS is to set the matrix to solid.
<br /> The purpose of the testing is for waste characterization and wastes,whether they are an oil,solid,or a liquid waste are typically
<br /> analyzed per SW 846 waste methodology-on a weight basis,so the data we reported is appropriate.
<br /> Except as noted below,all method specified calibrations and quality control performance criteria were met for this job.For more
<br /> information,please refer to QC summary pages.
<br /> Volatiles by GCMS By Method SW846 8260B
<br /> Matrix: SO Batch ID: VM1482
<br /> • Sample(s) C35719-5MS,C35719-5MSD were used as the QC samples indicated.
<br /> • Matrix Spike/Matrix Spike Duplicate Recovery(s)for 1,2,3-Trichlorobenzene, 1,2,4-Trichlorobenzene, 1,2,4-Trimethylbenzene,
<br /> 1,3,5-Trimethylbenzene,Acetone,Bromobenzene,Chloroethane,Di-Isopropyl ether,Hexachlorobutadiene,m-Dichlorobenzene,
<br /> n-Butylbenzene,n-Propylbenzene,Naphthalene,o-Dichlorobenzene,p-Chlorotoluene,p-Dichlorobenzene,p-Isopropyltoluene,
<br /> Styrene,trans-1,3-Dichloropropene are outside control limits. Probable cause due to matrix interference.
<br /> • C35685-I:Dilution required due to nature of sample matrix.
<br /> Extractables by GCMS By Method SW846 8270C
<br /> Matrix: SO Batch ID: OP10684
<br /> • Sample(s) C35683-IMS,C35683-IMSD were used as the QC samples indicated.
<br /> • Blank Spike Recovery(s)for 3,3'-Dichlorobenzidine,Benzidine,Benzoic acid are outside laboratory control limits(high bias):
<br /> not detected in associated samples.
<br /> • Matrix Spike/Matrix Spike Duplicate Recovery(s)for Benzidine,Chrysene are outside control limits.RPD(s)for MSD for
<br /> Benzidine are outside control limits for sample OP10684-MSD.Probable cause due to matrix interference.
<br /> • C35685-1:Dilution required due to matrix interference.Extract would not concentrate(dark and viscous);and high
<br /> concentration of non-target hydrocarbons. Surrogate recoveries for 2-Fluorophenol,Phenol-d5,Terphenyl-dl4 are outside
<br /> control limits due to dilution.
<br /> Extractables by GC By Method SW846 8015B M
<br /> Matrix: so Batch ID: OP10669
<br /> • Sample(s) C35705-14MS,C35705-14MSD were used as the QC samples indicated.
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