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Metals By Method SW846 6010B RECD JUL 24 2015 <br /> Matrix: SO Batch ID: MP8322 <br /> • Sample(s) C35683-IMS,C35683-1MSD,C35683-ISDL were used as the QC samples for metals. <br /> • Matrix Spike/Matrix Spike Duplicate Recovery(s)for Antimony,Barium,Zinc are outside control limits. Spike recovery <br /> indicates possible matrix interference and/or sample nonhomogeneity. <br /> • RPD(s)for MSD for Barium are outside control limits for sample MP8322-S2. High RPD indicates possible matrix <br /> interference and/or sample nonhomogeneity. <br /> • RPD(s)for Serial Dilution for Arsenic,Beryllium,Cadmium,Silver,Thallium are outside control limits for sample MP8322- <br /> SDI. Percent difference acceptable due to low initial sample concentration(<50 times IDL). <br /> • RPD(s)for Serial Dilution for Barium.Chromium,Copper,Lead.Vanadium,Zinc are outside control limits for sample <br /> MP8322-SDI. Serial dilution indicates possible matrix interference. <br /> Metals By Method SW846 7471A <br /> Matrix: SO Batch ID: MP8330 <br /> • Sample(s) C35683-IMSD,C35683-IMS were used as the QC samples for metals. <br /> • Matrix Spike Recovery(s)for Mercury are outside control limits. Spike recovery indicates possible matrix interference and/or <br /> sample nonhomogeneity. <br /> • C35685-1 for Mercury:Elevated reporting limit(s)due to matrix interference. <br /> Wet Chemistry By Method SW846 9071B <br /> Matrix: SO Batch ID: N:GP82674 <br /> • C35685-1 for HEM Oil and Grease:Analysis performed at Accutest Laboratories,Dayton,NJ. <br /> Wet Chemistry By Method SW846 CHAP? <br /> Matrix: SO Batch ID: N:GNIII17 <br /> • C35685-1 for Corrosivity as pH:Analysis performed at Accutest Laboratories,Dayton,NJ. <br /> Wet Chemistry By Method SW846 CHAP7/9012 B <br /> Matrix: SO Batch ID: N:GP82734 <br /> • C35685-1 for Cyanide Reactivity:Analysis performed at Accutest Laboratories,Dayton,NJ. <br /> Wet Chemistry By Method SW846 CHAP7/9034 <br /> Matrix: SO Batch ID: N:GP82733 <br /> • C35685-1 for Sulfide Reactivity:Analysis performed at Accutest Laboratories,Dayton,NJ. <br /> Wet Chemistry By Method SW846 CHAP?/ASTM D93 <br /> Matrix: SO Batch ID: N:GN11155 <br /> • C35685-1 for Ignitability(Flashpoint):Analysis performed at Accutest Laboratories,Dayton,NJ. <br /> Accutest Laboratories Northern California(ALNCA)certifies that this report meets the project requirements for analytical data <br /> produced for the samples as received at ALNCA and as stated on the COC.ALNCA certifies that the data meets the Data <br /> QualityObjectives for precision,accuracy and completeness as specified in the ALNCA Quality Manual except as noted above. <br /> This report is to be used in its entirety.ALNCA is not responsible for any assumptions of data quality if partial data packages are <br /> used <br /> Friday,September 05,2014 Page 2 of 2 <br /> ED 5 of 54 <br /> a ACCt-JTEST. <br /> C35685 .^'o...o. .. <br />