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1534 Willow Pass Road,Pith A 94565-1701 <br /> McCampbell AnalyMcal, Inc, Toll Free Telephone:(877)252-9262/Fax,(925)252-9269 <br /> r "N'lien Quality Coatis" hUp://www.morampbe0.mm/E-mail:man@ma ngilxa. <br /> QC SUMMARY REPORT FOR E418.1 <br /> WO Sample Matrix: Solid OC Matrix: Soil BatchlD:66339 WorkOrder: 1204148 <br /> EPA Method: E418.1 Extraction: SW3660 TRPH Spiked Sample ID: 1204116-001A <br /> Analyte <br /> Sample Spiked I MS MSD MS-MSD LCS Acceptance Criteria(%) <br /> mglKg mWKg %R. %Ree. %RPD %Rec. MS I MSD RPD I LCs <br /> TRPH 15,000 156 NR NR I NR 1 105 N/A I N/A 70-130 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: <br /> NONE <br /> BATCH 66339 SUMMARY <br /> Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date Extracted Date Analyzed <br /> 1204149-001A 04102/12 9:00 AM 04/06/12 04/12/12 1:05 PM <br /> MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Central Sample Duplicate;RPD=Relative Percent Deviation. <br /> %Recovery=100'(MS-Sample)I(Amount Spiked):RPD=100'(MS- MSD)I((MS+MSD)12). <br /> MS/MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons.a)the sample is inhomogenous AND contains <br /> significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. <br /> N/A=not enough sample to perform matrix spike and matrix spike duplicate. <br /> NR=analyte concentration in sample exceeds spike amount for sal matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. <br /> #six ate diluted out of range. <br /> DHS ELAP Certification 1644 QA/QC Officer <br /> Page 9 of 12 <br />