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t1tli 1534 Willow Pecs Road,Pith A 945651701 <br /> MCCampbell Analy (Cal, InC. ToO Free Teleph.:(877)252-9262/Fax:(925)252-9269 <br /> w y "When Quality Counts" http://www.morampbe0.cmr/E-mail main@mccmapbdtcom <br /> QC SUMMARY REPORT FOR SW6020 <br /> W.O.Sample Matrix: Solid QC Matra: Soil BatchlD:66360 WorkOrder: 1204148 <br /> EPA Method: SW6020 Extraction: SW8050B Spiked Sample ID: 1204074-001A <br /> AnalyteSample Spiked MS MSD MS-MSD LCS Acceptance Criteria(%) <br /> rnglKg mg/Kg %Ree. %Rec. %RPD %Rec. MS 1 MSD RPD LCS <br /> Antimony 0.84 50 95.5 95 0.557 98.2 75-125 20 75-125 <br /> Arsenic 12 50 102 104 1.12 111 75-125 20 75-125 <br /> Barium 70 501 105 103 1.56 106 75-125 20 75-125 <br /> Beryllium ND 50 94.1 93.9 0.255 99.7 75-125 20 75-125 <br /> Cadmium 2.6 50 98 97.1 0.876 102 75-125 20 75-125 <br /> Chromium 36 50 94.9 93.2 1.03 109 75-125 20 75-125 <br /> Cobalt 9.9 50 98 97.9 0.153 104 75-125 20 75-125 <br /> Copper 69 50 98.2 98 0.0849 113 75-125 20 75-125 <br /> Lead 71 50 111 105 Z41 101 75-125 20 75-125 <br /> Mercury 0.23 1.25 99 97.3 1.51 101 75-125 20 75-125 <br /> Molybdenum 1.3 50 106 104 1.82 108 75-125 20 1 75-125 <br /> Nickel 32 50 102 101 0.713 113 75-125 20 75-125 <br /> Selenium ND 50 1 98.7 100 1.30 111 75-125 20 75-125 <br /> Silver ND 50 927 92 0.845 95.8 75-125 20 75-125 <br /> Thallium ND 50 102 101 1.50 103 75-125 20 75-125 <br /> Vanadium 55 50 96.9 94.5 1.17 110 75-125 20 75-125 <br /> Zinc 180 501 96.4 96.6 0.180 108 1 75-125 20 75-125 <br /> -/.SS: 99 500 102 99 2.94 95 70-1301 20 70-130 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: <br /> NONE <br /> BATCH 66360 SUMMARY <br /> Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date Extracted Date Analyzed <br /> 120414MOIA 04/021129:00 AM 04/06/12 04/116:1211:39PM I 1204148-001A 04/02112 9:00 AM 04/06/12 04/09/127:23 PM <br /> MS=Matrix Spike,MSD=Maft Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Contra]Sample Duplicate;RPD=Relath x Percent Deviation. <br /> %Recovery=100'(MSSample)/(Amount Spiked);RPD=100'(MS- MSD)/((MS+MSD)/2). <br /> MS/MSD spike recoveries and I or%RPD may fall outside of laboratory acceptance criteda due to one or more of the following reasons:a)the sample is inhomogenous AND contains <br /> significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. <br /> N/A=not applicable to this method. <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2z spike amount for water matrhr or sant pie diluted due to high matrix or analyte content <br /> DHS ELAP Certification 1644 QA/QC Officer <br /> Page 10 of 12 <br />