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\tWi� 1534 Willow Peso Asad Pi A 945651701 <br /> Ma_Campbell Anply seal, Inc. Toll Free Telephore:(877)252-9262/Fax:(925)252-9269 <br /> "W "KIM Quakily Counts" Ldp://www.mccampbellcan/E mail:me.@m cm pb.]L. <br /> QC SUMMARY REPORT FOR SW8260B <br /> W.O.Sample Matrix: Solid QC Matrix: Soil BatchlD:66384 WorkOrder: 1204148 <br /> EPA Method: SW8260B Extraction: SW6030B Spiked Sample ID: 1204097-001A <br /> Analyte Sample Spiked MS MSD MS-MSD LCS Acceptance Criteria(%) <br /> mglV(q all %Rec. %Rec. %RPD %Rec. MS/MSD RPD LCS <br /> ted-Amyl methyl ether(TAME) ND 0.050 90.7 89.1 1.74 95.6 70-130 30 50-135 <br /> Benzene ND 0.050 108 106 1.83 109 70-130 30 70-137 <br /> t-Butyl alcohol(TBA) ND 0.20 97.4 95.5 1.93 95.8 70-130 30 50-143 <br /> Chlorobenzene ND 0.050 99.6 97.5 213 97.9 70-130 30 69-133 <br /> 1,2-DibromoctIme(EDB) ND 0.050 99.2 97.7 1.50 98.2 70-130 30 61-135 <br /> 1,2-Dichloroethane(1,2-DCA) ND 0.050 99 97.1 1.93 97.2 70-130 30 1 64-133 <br /> 1,1-Dichloroethene ND 0.050 102 1 101 0.984 1 101 70-130 30 70-142 <br /> Diisopropyl ether(RIPE) ND 0.050 982 96.3 1.92 97.3 70-130 30 65-134 <br /> Ethyl ted-butyl ether(ETBE) ND 0.050 97.6 95.1 2.53 95.9 70-130 30 61-127 <br /> Methyl-t-butyl ether(MTBE) ND 0.050 97.8 95.5 238 96.1 70-130 30 65-130 <br /> Toluene ND 0.050 110 107 295 107 70-130 30 70-146 <br /> Trichloroethene ND 0.050 106 105 1.43 106 70-130 30 66-143 <br /> %SSI: 91 0.12 101 102 0.903 100 70-130 30 70-130 <br /> %SS2: 102 0.12 108 108 0 108 70-130 30 70-130 <br /> %SS3: 88 1 0.012 101 1 101 1 0 1 103 70-130 1 30 1 70-130 <br /> All target compounds in the Method Blank ofthis extraction batch were ND leas than the method RL with the following exceptions: <br /> NONE <br /> BATCH 66384 SUMMARY <br /> Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date Extracted Date Analyzed <br /> 1204148-001A 04/02/12 9:00 AM 04/06/12 04/10/1211:03 PM <br /> MS=Matrix Spike;MSD=Mabbt Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate;RPD=Relative Percent Deviation. <br /> %Recovery=100'(MSSample)/(Amount Spiked);RPD=100'(MS- MSD)/((MS+MSD)/2). <br /> MS/MSD spike recoveries and/or%RPD may tall outside of laboratory acceptance criteria due to one or mare of the following reasons:a)the sample is inhomogenous AND contains <br /> significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's mats interferes with the spike rew✓ery. <br /> N/A=not enough sample to perform matrix spike and matrix spike duplicate. <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte cement. <br /> Laboratory extraction solvents such as methylene chloride and acetone may occasionally appear in the method blank at low levels. <br /> DHS ELAP Certification 1644 QA/QC Officer <br /> Page 11 of 12 <br />