|
X
<br />KEROSENE X X
<br />UNK FUEL X X X X X
<br />X
<br />PROD. OIL X X
<br />CHLOR. X
<br />SOLVENTS X X
<br />NONCHLOR II I I — I I I X
<br />WASTE\ X X
<br />USED OIL X X
<br />X
<br />ii found i
<br />All analysis methods are the designated EPA methods described in EPA
<br />SW 846. ThandixtD (B), Table 3 5 on pagetion. Those methods tA20 fob
<br />846 are specifically noted below. Refer to the "SWRCB LUFT Field Manual", Appe
<br />minimum detection limits for motor vehicle fuel (gasoline and diesel). Refer to "Tri -Regional Board Staff Recommendatiq_"
<br />Initial Evaluation and Investigation of UST's" for the waste and motor oil minimum detection limits.
<br />Detection Limits that remain below the MCL, STLC or Allowable Limit of the contaminant in question will be accepted,
<br />however laboratory shall utilize the most conservative method.
<br />LABORATORY ANALYSES TERMINOLOGY:
<br />Total Petroleum Hydrocarbon, Gasoline, GC/FID (5030) 8015 mod or GC/MS 8260
<br />TPH-G
<br />Total Petroleum Hydrocarbon, Diesel, GC/FID (3550), 8015 mod or GCIMS 8260
<br />VERIFICATION LABORATORY ANALYSIS
<br />Benzene, Toluene, Xylene & Ethyl Benzene, GC/PID 8020 or GC/MS 8260
<br />BTX & E
<br />DilNT�ILn1
<br />CL HC
<br />TOTAL LEAD
<br />Total lead, AA 7420, AA 7421 or ICP -AES 6010 ,
<br />ETBE, TAME, DIPE, & TBA GCIMS 8260 (For MTBE screen only you may use 8(20)
<br />7000.
<br />OXYGENATES
<br />AA
<br />MTBE,
<br />Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption Spectrometry
<br />O.WGENATES
<br />Metals: Cadmium, Chromium III and VI, Lead, Zinc and Nickel.
<br />TANK TPH-G TPH-D BTX & E CL HC TOTAL MTBE
<br />(MTBE.
<br />TBA.DIPE.
<br />n�rnu B
<br />ICAPi 5270
<br />TANK
<br />8015 8015 8020 8010 LEAD 8020
<br />ETBE.
<br />AES 8080
<br />pCONTENTS
<br />8260 8260 8260 8240 7420 8260
<br />TAME)
<br />or
<br />8260 7421
<br />Method 5030
<br />AA
<br />LEADED GAS X X X
<br />rtr.[t rcc X X
<br />X
<br />X
<br />I
<br />X
<br />KEROSENE X X
<br />UNK FUEL X X X X X
<br />X
<br />PROD. OIL X X
<br />CHLOR. X
<br />SOLVENTS X X
<br />NONCHLOR II I I — I I I X
<br />WASTE\ X X
<br />USED OIL X X
<br />X
<br />ii found i
<br />All analysis methods are the designated EPA methods described in EPA
<br />SW 846. ThandixtD (B), Table 3 5 on pagetion. Those methods tA20 fob
<br />846 are specifically noted below. Refer to the "SWRCB LUFT Field Manual", Appe
<br />minimum detection limits for motor vehicle fuel (gasoline and diesel). Refer to "Tri -Regional Board Staff Recommendatiq_"
<br />Initial Evaluation and Investigation of UST's" for the waste and motor oil minimum detection limits.
<br />Detection Limits that remain below the MCL, STLC or Allowable Limit of the contaminant in question will be accepted,
<br />however laboratory shall utilize the most conservative method.
<br />LABORATORY ANALYSES TERMINOLOGY:
<br />Total Petroleum Hydrocarbon, Gasoline, GC/FID (5030) 8015 mod or GC/MS 8260
<br />TPH-G
<br />Total Petroleum Hydrocarbon, Diesel, GC/FID (3550), 8015 mod or GCIMS 8260
<br />TPH-D
<br />Benzene, Toluene, Xylene & Ethyl Benzene, GC/PID 8020 or GC/MS 8260
<br />BTX & E
<br />Chlorinated Hydrocarbon, GC/HSD 8010, GC/IvIS 8240 or 8260
<br />CL HC
<br />TOTAL LEAD
<br />Total lead, AA 7420, AA 7421 or ICP -AES 6010 ,
<br />ETBE, TAME, DIPE, & TBA GCIMS 8260 (For MTBE screen only you may use 8(20)
<br />7000.
<br />OXYGENATES
<br />AA
<br />MTBE,
<br />Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption Spectrometry
<br />METALS ICAP or
<br />Metals: Cadmium, Chromium III and VI, Lead, Zinc and Nickel.
<br />PCB
<br />Polychlorinated Biphenyls, GC/MS 8270 or 8080
<br />GC -FID
<br />Gas Chromatography, Flame Ionization Detection
<br />Method 3050
<br />Acid dieestion
<br />Method 3510
<br />Soxhiet sample preparation
<br />preparation, extraction method
<br />Method 3550
<br />Sonication sample
<br />Method 5030
<br />Purge and trap sample preparation
<br />QA/QC
<br />Quality Assurance/Quality Control
<br />benzene -free solvents are to be used. Fused capillary columns are preferred to packed
<br />Notes: To avoid false positive detection of benzene,
<br />be as a "first cut" with "dirty" samples or once the hydrocarbons have been characterized and proper
<br />columns: a packed column
<br />may used
<br />QA/QC is followed.
<br />sources,
<br />EPA recommends that the 500 series for volatile organic should be used in preference to the G00 caries because the
<br />may require further analysis.
<br />For drinking water
<br />detection limits are lower and the QA/QC is better. Samples exhibiting any level of heavy metal contamination
<br />PHS-EHD recommends holding those samples until disposal is indicated.
<br />EH 23 046 (Revised 05/09100) 1 Page 8
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