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li <br /> MINIA,._,, VERIFICATION LABORATORY ANAL. ... <br /> METALS PCB <br /> TANK TANK TPH-G TPH-D BTX & E CL HC TOTAL ICRP/ 8270 <br /> # CONTENTS 8015 8015 8020 8010 LEAD AES or 8080 <br /> 8260 8260 8260 8240 7420 AA <br /> XLEADED X X <br /> GAS X <br /> UNL GAS X X <br /> DIESEL X X <br /> KEROSENE X X <br /> UNK FUEL X X X X <br /> PROD. OIL X X <br /> CHLOR. <br /> SOLVENTS X X <br /> NONCHLOR X <br /> SOLVENTS X X <br /> WASTE\ X X X <br /> USED OIL X X T7:X <br /> All analyses methods are designated EPA methods described in EPA SW 846, Third Edition. Those methods act found <br /> in SW 846, are specifically noted below. Refer to the "SWRCB LUFT Field Manual", Appendix A-20, Table 3-5 for <br /> detection limits of motor vehicle fuels (gasoline and diesel). Refer to 1-2-3 "Regional Board Staff Recommendations for <br /> Initial Evaluation and Investigation of UST's" for the waste and motor oil detection limits. <br /> I)election Limits that remain below the MCI, STLC or Allowable Limit of the contaminant In question will be accepted, <br /> however laboratory shall utilize lire most conservative method. <br /> LABORATORY ANALYSES TERMINOLOGY: <br /> TMI_G Total Petroleum Hydrocarbon, Gasoline, GC/FID (5030) 8015 mod or GC/MS 8260 <br /> TPFI-D Total Petroleum Hydrocarbon, Diesel, GC/FID (3550), 8015 mod or GUMS 8260 <br /> DTX & E Benzene, Toluene, Xylene Bei Ethyl Benzene, GC/PID 8020 or GC/MS 8260 <br /> CL HC Chlorinated Hydrocarbon, GC/HSD 8010, GUMS 8240 <br /> TOTAL LEAD Total lead, AA 7420, AA 7421 or ICP-AES 6010 <br /> EDB Ethylene dibromide (DHS-AB 1803), GC/MS 8240 (DHS-LUFT) <br /> GC-FID Gas Chromatography, Flame Ionization Detection <br /> ICAP or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption <br /> Spectrometry 7000. Metals: Cadmium ,Chromium III and VI, Lead, Zinc and Nickel. <br /> l <br /> PCB Polychlorinated Biphenyls, GC/MS 8270 or 8080 <br /> Method 3050 Acid digestion <br /> Method 3540 Soxhlet sample preparation <br /> Method 3550 Sonication sample preparation, extraction method <br /> Method 5030 Purge and trap sample preparation <br /> QA/QC Quality Assurance/Quality Control <br /> Notes: To avoid false positive detection of benzene, benzene-free solvents are to be used. Fused capillary columns are <br /> preferred to packed columns; a packed column may be used as a "first cut" with "dirty" samples or once the hydrocarbons <br /> have been characterized and proper QA/AC is followed. <br /> For Drinking water sources, EPA recommends that the 500 series for volatile organics be used In preference to the 600 <br /> series because the detection limits are lower and the QA/QC is better. Samples exhibiting any level of heavy metal <br /> contamination may require further analysis. PHS-EHD recommends holding these samples until disposal Is indicated. <br /> Ell 23 048 (Revised 7/10/92) Page 8 <br />