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110 Second Avenue South, #D7, Pacheco, CA 94553 <br />14 McCAMPBELL ANALYTICAL INC. Telephone: 510-798-1620 Fax : 510-798-1622 <br />htto://www.mccamobell.com E-mail: main@mccampbell.com <br />Advanced GeoEnviromnental <br />1803 West March Lane, Ste A <br />Stockton, CA 95207 <br />Client Project ED: Cherokee Truck Stop <br />Date Sampled: 09/18-09/22/97 <br />Date Received: 09/23/97 <br />Client Contact: Kevin McKibben <br />Date Extracted: 09/24/97 <br />Client P.O: <br />Date Analyzed: 09/24-09/29/97 <br />EPA method 8260 <br />Volatile Organics By GC/MS <br />Lab ID <br />81033 <br />Client lD <br />p-5 <br />Matrix <br />S <br />Compound Concentration• <br />Compound <br />Concentration' <br />Acetone <br />Benzene <br />ND<200 <br />4300 <br />trans-1,3-Dic"Oro propene <br />Ethylene dibromide' <br />ND<200 <br />ND<200 <br />Brornobenzene <br />ND<200 <br />Ethylbenzene <br />Bromochloromethane <br />ND<200 <br />Hexachlorobutadiene <br />Bromodichloromethane <br />ND<200 <br />lodomethane <br />Bromoform <br />ND<200 <br />Isopropylbenzene <br />:UND<2 <br />Bromomethane <br />ND<200 <br />p -Isopropyl toluene <br />n -Butyl benzene <br />ND<200 <br />Methyl butyl ketone "' <br />sec -Butyl benzene <br />ND<200 <br />Methylene Chloride" <br />ND<200 <br />tert-Butyl benzene <br />ND<200 <br />Methyl ethyl ketones <br />ND<200 <br />Carbon Disulfide <br />ND<200 <br />Methyl isobutyl ketone" <br />ND<200 <br />Carbon Tetrachloride <br />ND<200 <br />Methyl tert-Butyl Ether (MTBE) <br />--- <br />Chlorobenzrne <br />ND<200 <br />Napthalene <br />ND<200 <br />Chloroethane <br />ND<200 <br />n -Propyl benzene <br />620 <br />2-Chlorcethyl Vinyl Ether" <br />ND<200 <br />Styrene "I <br />ND<200 <br />Chloroform <br />9D<200 <br />1,1,1,2 -Tetrachloroethane <br />ND<200 <br />Chloromethane <br />ND<200 <br />1,1,2,2 -Tetrachloroethane <br />ND<200 <br />2-Chlorotolurne <br />ND<200 <br />Tetrachloroethene <br />ND<200 <br />4-Chlorotoluene <br />ND<200 <br />Toluene""' <br />ND<200 <br />Dibromochloromethane <br />ND<200 <br />1,2,3-Tiichlorobenzene <br />ND<200 <br />1,2-Dibromo-3-chloropropane <br />ND<200 <br />1,2,4-Trichlorobenzene <br />ND<200 <br />Dibromomethane <br />ND<200 <br />1,1,1 -Trichloroethane <br />ND<200 <br />1,2 -Dichlorobenzene <br />ND<200 <br />1,1,2 -Trichloroethane <br />ND<200 <br />1,3 -Dichlorobenzene <br />ND<200 <br />Trichloroethene <br />ND<200 <br />1,4 -Dichlorobenzene <br />ND<200 <br />Trichlorofluoromethane <br />ND<200 <br />Dichlorodifluoromethane <br />ND<200 <br />1,2,3-Trichloropropane <br />ND<200 <br />]J-Dichlorcethane <br />ND<200 <br />1,2,4-Trimethylbenzene <br />ND<200 <br />1,2-Dichlomethane <br />ND<200 <br />1,3,5-Trimethylbenzene <br />ND<200 <br />1,1-Dichlorcethene <br />ND<200 <br />Vinyl Acetate`" <br />ND<200 <br />cis-1,2-Dichloroethene <br />ND<200 <br />Vinyl Chloride "" <br />ND<200 <br />trans-12-Dichloroethene <br />ND<200 <br />Xylenes, total "" <br />230 <br />1,2-Dichloropropane <br />ND<200 <br />Comments: <br />1,3-Dichloropropane <br />ND<200 <br />Surrogate Recoveries ('V,.) <br />2,2-Dichloropmpane <br />ND<200 <br />Dibromofluoromethane <br />85 <br />),l-Dichloropropene <br />ND<200 <br />Toluene -d8 <br />89 <br />cis-1,3-Dichloropropene I <br />ND<200 <br />4-13romofluorobenzene <br />83 <br />water and vapor samples are reported in ug/L, soil and sludge samples in ug/kg, wipes in ug/wipe and all TCLP / SPLP extracts in ug/L <br />Reporting limits unless otherwise stated: water samples 1 ug/L; vapor samples 0.5 ug/L; solid and sludge samples 5 ug/kg; wipes 0.2ug/wipe <br />ND means not detected above the reporting limit; N/A means analyte not applicable to this analysis <br />(b) 2-propanone or dimethyl ketone; (c) (2chlorcethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br />pentanone or isopropylacetone; (h) lighter than water immiscible sheen is present; (i) liquid sample that contains greater than —5 vol. % <br />sediment; 0) sample diluted due to high organic content, (k) ethenylbenzene; 0) methylbenzene; (m) acetic acid ethenyl ester; (n) <br />chloroethene; (o) dimethylbenzenes. <br />DHS Certification No. 1644 //Edward Hamilton, Lab Director <br />