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u <br />110 Second Avenue South, #D7, Pacheco, CA 94553 <br />McCAMPBELL ANALYTICAL INC. Telephone : 510-798-1620 Fax : 510-798-1622 <br />http://www.mccami)bell.com E-mail: main@mccampbell.com <br />Advanced GeoEnvironmental <br />1803 West March Lane, Ste A <br />Stockton, CA 95207 <br />Client Project ID: Cherokee Truck Stop <br />Date Sampled: 09/18-09/22/97 <br />Date Received: 09/23/97 <br />Client Contact: Kevin McKibben <br />Date Extracted: 09/24/97 <br />Client P.O: <br />Date Analyzed: 09/24-09/29/97 <br />EPA method 8260 <br />Volatile Organics By GC/MS <br />Lab ID <br />81036 <br />Client ID <br />P-8 <br />Matrix <br />S <br />Compound <br />Concentration* <br />Compound <br />Concentration` <br />Acetone t <br />ND<I2 <br />trans-1,3-Diclilompropene <br />ND <br />Benzene <br />7.0 <br />Ethylene dibromide' <br />ND <br />Bromobenzene <br />ND <br />Ethylbenzene <br />8.9 <br />Bromochloromethane <br />ND <br />Hexachlorobumdiene <br />ND <br />Bromodichloromethane <br />ND <br />lodmnethane <br />ND <br />Bromoform <br />ND <br />Isopmpylbenzene <br />5.1 <br />Bromomethane <br />ND <br />p4sopropyl toluene <br />ND <br />n -Butyl benzene <br />9.1 <br />Methyl butyl ketone"' <br />ND <br />sec -Butyl benzene <br />7.3 <br />Methylene Chloride' <br />ND <br />tert-Butyl benzene <br />ND <br />Methyl ethyl ketone"' <br />ND <br />Carbon Disulfide <br />ND <br />Methyl isobutyl ketone <br />ND <br />Carbon Tetrachloride <br />ND <br />Methyl tert-Butyl Ether (MTBE) <br />--- <br />Chlorobenzene <br />ND <br />Napthalene <br />ND <br />Chloroethane <br />ND <br />n -Propyl benzene <br />15 <br />2-Chloroethyl Vinyl Ether` <br />ND <br />Styrene "' <br />ND <br />Chloroform <br />ND <br />1.1,1,2 -Tetrachloroethane <br />ND <br />Chloromethane <br />ND <br />1,1,2.2 -Tetrachloroethane <br />ND <br />2-Chlorotoluene <br />ND <br />Tenachloroethene <br />ND<8 <br />4-Chlorotoluene <br />ND <br />Toluene""' <br />36 <br />Dibromochloromethane <br />ND <br />1.2,3-Trichlorobenzene <br />ND <br />1,2-Dibromo-3-chlompropane <br />ND <br />1.2,4-Trichlorobenzene <br />ND <br />Dibromometbane <br />ND <br />1,1,1-Trichloroeth3ne <br />ND <br />1,2 -Dichlorobenzene <br />ND <br />1,1,2 -Trichloroethane <br />ND <br />1,3 -Dichlorobenzene <br />ND <br />Trichloroethene <br />ND <br />1,4 -Dichlorobenzene <br />ND <br />Trichlorofluoromethane <br />ND <br />Dichlorodifluoromethane <br />ND <br />1,2,3-Trichloropropane <br />ND <br />1,1-Dichloroethane <br />ND <br />1,2,4-Trinxthylbenzene <br />7.4 <br />1,2-Dichloroethane <br />ND <br />1,3.5-Trinvihylbenzene <br />ND <br />IJ-Dichloroethene <br />ND <br />Vinyl Acetate "' <br />ND <br />cis-1,2-Dichloroethene <br />ND <br />Vinyl Chloride " <br />ND <br />trans-1,2-Diebloreethene <br />ND <br />Xylenes,total 'P <br />43 <br />1,2-Dichloropropane <br />ND <br />Comments: <br />1,3-Dichloropropane <br />ND <br />Surrogate Recoveries (%) <br />2,2-Dichloropropane <br />ND <br />Dibromofluormnethane <br />100 <br />1,1-Dichloropropene <br />ND <br />Toluene -d8 <br />101 <br />cis-1,3-Diebloropropme <br />ND <br />4-Bromofluorobenzene <br />93 <br />water and vapor samples are reported in ug/L, soil and sludge samples in ug/kg, wipes in ug/wipe and all TCLP / SPLP extracts in ug/L <br />Reporting limits unless otherwise stated: water samples 1 ug/L; vapor samples 0.5 ug/L; solid and sludge samples 5 ug/kg; wipes 0.2ug/wipe <br />ND means not detected above the reporting limit; N/A means analyte not applicable to this analysis <br />(b) 2-propanone or dimethyl ketone; (c) (2chlomethoxy) ethene; (d) 2-hexxnone; (e) dichloromethane; (f) 2-bumnone; (g) 4•methyl-2- <br />pentanone or isopropylacetone; (h) lighter than water immiscible sheen is present; (i) liquid sample that contains greater than —5 vol. % <br />sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene, (m) acetic acid cthenyl ester; (n) <br />chlomethene;(o) dimethylbenzenes. <br />DHS Certification No. 1644 Z Edward Hamilton, Lab Director <br />