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'r <br />... <br />110 Second Avenue South, #D7, Pacheco, CA 94553 <br />14 1 McCAMPBELL ANALYTICAL INC. Telephone : 510-798-1620 Fax : 510-798-1622 <br />htto://www.mccanipbell.com E-mail: main@mccampbell.com <br />Advanced GeoEnvironmental <br />1803 West March Lane, Ste A <br />Stockton, CA 95207 <br />Client Project ID: Cherokee Truck Stop <br />Date Sampled: 09/18-09/22/97 <br />Date Received: 09/23/97 <br />Client Contact: Kevin McKibben <br />Date Extracted: 09/24/97 <br />Client P.O: <br />Date Analyzed: 09/24-09/29/97 <br />EPA method 8260 <br />Volatile Organics By GC/MS <br />Lab ID <br />81041 <br />Client ID <br />P-13 <br />Matrix <br />S <br />Compound Concentration* <br />Compound <br />Concentration* <br />Acetone <br />ND<480 <br />trans-13-Dichlompropene <br />ND<340 <br />Benzene <br />ND<340 <br />Ethylene dibromide' ' <br />ND<340 <br />Bromobenzene <br />ND<340 <br />Ethylbenzene <br />1500 <br />Bromochloromethane <br />ND<340 <br />Hexachlorobutadiene <br />ND<340 <br />Bromodichloromethane <br />ND<340 <br />lodomethane <br />ND<340 <br />Bromoform <br />ND<340 <br />Isopropylbenzene <br />1100 <br />Bromomethane <br />ND<340 <br />p -Isopropyl toluene <br />ND<340 <br />n -Butyl benzene <br />5200 <br />Methyl butyl ketone "' <br />ND<340 <br />sec -Butyl benzene <br />1500 <br />Methylene Chloride... <br />ND<440 <br />tert-Butyl benzene <br />1500 <br />Methyl ethyl ketone'{' <br />ND<340 <br />Carbon Disulfide <br />ND<340 <br />Methyl isobutyl ketone <br />ND<340 <br />Carbon Tetrachloride <br />ND<340 <br />Methyl tert-Butyl Ether (MTBE) <br />--- <br />Chlorobenzene <br />ND<340 <br />Napthalene <br />ND<430 <br />Chloroethane <br />ND<340 <br />n -Propyl benzene <br />2900 <br />2-Chloroet1hyl Vinyl Ether"' <br />ND<340 <br />Styrene <br />ND<340 <br />Chloroform <br />ND<340 <br />1.1,1,2 -Tetrachloroethane <br />ND<340 <br />Chloromethane <br />ND<340 <br />1,1,2,2 -Tetrachloroethane <br />ND<340 <br />2-Chlorotoluene <br />ND<340 <br />Tetrachlorcethene <br />ND<530 <br />4-Chlorotoluene <br />ND<340 <br />Toluene"" <br />440 <br />Dibromochloromethane <br />ND<340 <br />1,2,3-Trichlorobenzene <br />ND<340 <br />1,2-Dibromo-3-ehlompropane <br />ND<340 <br />1,2,4-Trichlorobenzene <br />ND<340 <br />Dibromomethane <br />ND<340 <br />1,1,1 -Trichloroethane <br />ND<340 <br />1,2 -Dichlorobenzene <br />ND<340 <br />1,1,2 -Trichloroethane <br />ND<340 <br />1,3-Dichlorobenzme <br />ND<340 <br />Trichloroethene <br />ND<340 <br />1,4 -Dichlorobenzene <br />ND<340 <br />Trichlorofluoromethane <br />ND<340 <br />Dichlorodifluoromethane <br />ND<340 <br />1.2,3 -T) <br />ND<340 <br />]J-Dichlorcethane <br />ND<340 <br />1,2,4-Trinxthylbenzene <br />8200 <br />1,2-Dichloroethane <br />NDC340 <br />1,3,5 -Tri methylbenzene <br />2500 <br />1,1-Dichloroethene <br />ND<340 <br />Vinyl Acetate "" <br />ND<340 <br />cis-1,2-Dlehlomethene <br />ND<340 <br />Vinyl Chloride" <br />ND<340 <br />trans-1,2-INchloroethene <br />ND<340 <br />Xylenes, total <br />5800 <br />1,2-Dichloropropane <br />ND<340 <br />Comments: <br />1,3-Dichloropropane <br />ND<340 <br />Surrogate Recoveries (% ) <br />2,2-Dichloropropane <br />ND<340 <br />Dibromofluoromethane <br />85 <br />1,1-Dichlompropene <br />ND<340 <br />Toluene -d8 <br />94 <br />cis-1,3-Dichloropropene <br />ND<340 <br />4-Bromotluorobenzene <br />90 <br />water and vapor samples are reported in ug/L, soil and sludge samples in ug/kg, wipes in ug/wipe and all TCLP / SPLP extracts in ug/L <br />Reporting limits unless otherwise stated: water samples 1 ug/L; vapor samples 0.5 ug/L; solid and sludge samples 5 ug/kg; wipes 0.2ug/wipe <br />ND means not detected above the reporting limit; N/A means analyte not applicable to this analysis <br />(b) 2-propanone or dimethyl ketone; (c) (2-chlorcethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (t) 2-butanone; (g) 4-methyl-2- <br />pentanone or isopropylacetone; (h) lighter than water immiscible sheen is present; (i) liquid sample that contains greater than —5 vol. % <br />sediment; 6) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br />chloroethene;(o) dimethylbenzenes. <br />DHS Certification No. 1644 /� Edward Hamilton, Lab Director <br />