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110 Second Avenue South, #D7, Pacheco, CA 94553 <br />MCCAWBELL ANALYTICAL INC. Telephone : 510-798-1620 Fax : 510-798-1622 <br />http://www mecamobell com E-mail: main@mccampbell.com <br />Advanced GeoEnvironmental <br />1803 West March Lane, Ste A <br />Stockton, CA 95207 <br />Client Project ID: Cherokee Truck Stop <br />Date Sampled: 09/18-09/22/97 <br />Date Received: 09/23/97 <br />Client Contact: Kevin McKibben <br />Date Extracted: 09/24/97 <br />Client P.O: <br />Date Analyzed: 09/24-09/29/97 <br />Volatile Organics By GC/MS <br />E�thhod <br />ELab ID <br />81043 <br />ent ID <br />T2 -E <br />trix <br />S <br />Compound <br />Concentration• <br />Compound <br />Concentration` <br />Acetone' <br />ND<2500 <br />trans-1,3-Dichloropropene <br />ND<2500 <br />Benzene <br />8700 <br />Ethylene dibromide' <br />ND<2500 <br />Bromobenzene <br />Bromochlorome[hane <br />ND<2500 <br />ND<2500 <br />Ethylbenzene <br />Hexachlorobutadiene <br />35,000 <br />ND<2500 <br />Bmmodichlommethane <br />ND<2500 <br />]odomethane <br />ND<2500 <br />Bromoform <br />ND<2500 <br />Isopropylbenzene <br />6700 <br />Bromomethane <br />7D<2500 <br />p -Isopropyl toluene <br />ND<2500 <br />n -Butyl benzene <br />15,000 <br />Methyl butyl ketone "' <br />ND<2500 <br />sec -Butyl benzene <br />4700 <br />Methylene Chloride"' <br />ND<3500 <br />tert-Butyl benzene <br />7000 <br />Methyl ethyl ketones' <br />ND<2500 <br />Carbon Disulfide <br />ND<2500 <br />Methyl isobutyl ketone' <br />ND<2500 <br />Carbon Tetrachloride <br />ND<2500 <br />Methyl tert-Butyi Ether (MTBE) <br />-- <br />Chlorobenzene <br />ND<2500 <br />Napthalene <br />ND<2500 <br />Chloroethane <br />ND<2500 <br />n -Propyl benzene <br />18,000 <br />2-Chlormthyl Vinyl Ether` <br />ND<2500 <br />Serene ' <br />ND<2500 <br />Chloroform <br />ND<2500 <br />1.1,1,2 -Tetrachloroethane <br />ND<2500 <br />Chloromethane <br />ND<2500 <br />1,1,2,2 -Tetrachloroethane <br />ND<2500 <br />2-Chlorotolume <br />ND<2500 <br />Tetrachloroethene <br />ND<3300 <br />4-Chlorotoluene <br />ND<2500 <br />Toluene "' <br />3100 <br />Dibromochloromethane <br />ND<2500 <br />1,2.3-Trichlorobenzene <br />ND<2500 <br />1,2-Dibromo-3-ebloropropane <br />ND<2500 <br />1,2,4-Trichlorobenzene <br />ND<2500 <br />Dibromomethane <br />ND<2500 <br />1,1,1 -Trichloroethane <br />ND<2500 <br />1,2 -Dichlorobenzene <br />NIX2500 <br />1,1,2 -Trichloroethane <br />ND<2500 <br />1,3 -Dichlorobenzene <br />ND<2500 <br />Trichloroethene - <br />ND<2500 <br />1,4 -Dichlorobenzene <br />ND<2500 <br />Trichlorofluoromethane <br />ND<2500 <br />Dichlorodifluoromethane <br />ND<2500 <br />1,2,3-Trichloropropane <br />ND<2500 <br />l,l-Dichloroethane <br />ND<2500 <br />1,2,4-Trimethylbenzene <br />72,000 <br />1,2-Dichloroethane <br />ND<2500 <br />1,3,5-Trimethylbenzene <br />20,000 <br />1, 1 -Dichlormthene <br />ND<2500 <br />Vinyl Acetate"" <br />3500 <br />cis-1,2-Dichlormthene <br />ND<2500 <br />Vinyl Chloride '°' <br />N5Q500 <br />trans-1,2-Dichloroethene <br />NIX2500 <br />Xylenes. total <br />69,000 <br />1,2-Dichloropmpane <br />ND<2500 <br />Comments: <br />1,3-Diehloropmpane <br />ND<2500 <br />Surrogate Recoveries ("/„) <br />2,2-Dichloropropane <br />ND<2500 <br />Dibromofluoromethane 84 <br />IJ-Dichloropropene <br />NIX2500 <br />Toluene -d8 96 <br />cis-1,3-Dichloropropene <br />ND<2500 <br />4-Bromofluorobenzene 84 <br />water and vapor samples are reported in ug/L, soil and sludge samples in ug/kg, wipes in ug/wipe and all TCLP / SPLP extracts in ug/L <br />Reporting limits unless otherwise stated: water samples I ug/L; vapor samples 0.5 ug%L: solid and sludge samples 5 ug/kg; wipes 0.2ug/wipe <br />ND means not detected above the reporting limit; N/A means analyte not applicable to this analysis <br />(b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br />pentanone or isopropylacetone; (h) lighter than water immiscible sheen is present; (i) liquid sample that contains greater than —5 vol. <br />sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br />chloroethene; (o) dimethylbenzenes. <br />DHS Certification No. 1644 <br />//—Edward Hamilton, Lab Director <br />