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INI <br />110 Second Avenue South, #D7, Pacheco, CA 94553 <br />McCAMPBELL ANALYTICAL INC. Telephone .510 <br />s 10-798-1620 Fax :510-798-1622 <br />http://www.mccampbell.com E-mail: main@mccampbelf.com <br />GeoEnvironmental <br />1803 West March Lane, Ste A <br />Stockton, CA 95207 <br />Client Project ID: Cherokee Truck Stop <br />Date Sampled: 09/18-09/22/97 <br />Date Received: 09/23/97 <br />Client Contact: Kevin McKibben <br />Date Extracted: 09/24/97 <br />Client P.O: <br />Date Analyzed: 09/24-09/27/97 <br />EPA method 6260 <br />Volatile Organics By GC/MS <br />81048 <br />jLabD <br />t ID <br />T5 -E <br />x <br />S <br />Compound Concentration* <br />Compound <br />Concentration* <br />Acetone' <br />ND<26 <br />trans-1,3-Dichloropropene <br />ND <br />Benzene <br />ND <br />Ethylene dibromide' ' <br />ND <br />Bronnbenzene <br />ND <br />Ethylbenzene <br />ND <br />Bromochloromethane <br />ND <br />Hexachlorobutodiene <br />ND <br />Bromodichloromethane <br />ND <br />Iodomethane <br />ND <br />Bromoform <br />ND <br />Isopropylbenzene <br />ND <br />Bromomethane <br />ND <br />p -Isopropyl toluene <br />ND <br />n -Butyl benzene <br />ND <br />Methyl butyl ketone "' <br />ND <br />sec -Butyl benzene <br />ND <br />Methylene Chloride" <br />ND <br />tert-Butyl benzene <br />ND <br />Methyl ethyl ketone'°' <br />ND <br />Carbon Disulfide <br />ND <br />Methyl isobutyl ketone <br />ND <br />Carbon Tetrachloride <br />ND <br />Methyl ten -Butyl Ether (MTBE) <br />— <br />Chlorobenzene <br />ND <br />Napthalene <br />ND <br />Chloroethane <br />ND <br />n -Propyl benzene <br />ND <br />2-Chloroethyl Vinyl Ethe <br />ND <br />Styrene <br />ND <br />Chloroform <br />ND <br />1,1,12 -Tetrachloroethane <br />ND <br />Chloromethane <br />ND <br />1,1.2,2 -Tetrachloroethane <br />ND <br />2-Chlorotoluene <br />ND <br />Tetrachloroethene <br />ND<8 <br />4-Chlorotoluene <br />ND <br />7oluene- <br />ND <br />Dibromochloremethane <br />ND <br />12,3-Trichlorobenzene <br />ND <br />1,2-Dibromo-3-ebloropropane <br />ND <br />12,4-Trichlorobenzene <br />ND <br />Dibromomethane <br />ND <br />1,1,1 -Trichloroethane <br />ND <br />12 -Dichlorobenzene <br />ND <br />1,1.2 -Trichloroethane <br />ND <br />1,3 -Dichlorobenzene <br />ND <br />Trichloroethene <br />ND <br />1,4 -Dichlorobenzene <br />ND <br />Trichlorofluoromethane <br />ND <br />Dichlorodifluoromethane <br />ND <br />1.2,3-Trichloropropane <br />ND <br />1,1-Dichloreethane <br />ND <br />12,4-Trimethylbenzene <br />ND <br />1,2-Dichlormthane <br />ND <br />1.3.5-Trimethylbenzene <br />ND <br />1,1-Dichloroethene <br />ND <br />Vinyl Acetate "" <br />ND <br />cis-1,2-Dichloroethene <br />ND <br />Vinyl Chloride 101 <br />ND <br />trans-1,2-Dichloroethene <br />ND <br />Xylenes, total 1p <br />ND <br />1,2-Dichloropmpane <br />ND <br />Comments: <br />1,3-Dichloropropane <br />ND <br />Surrogate Recoveries (% ) <br />2,2-Dichloropmpane <br />ND <br />Dibromolluoromethane <br />86 <br />1,1-Dichloropropene <br />ND <br />Toluene -d8 <br />99 <br />cis-1,3-Dichloropropene <br />ND <br />4-Bromolluorobenzene <br />90 <br />water and vapor samples are reported in ug/L, soil and sludge samples in ug/kg, wipes in ug/wipe and all TCLP / SPLP extracts in ug/L <br />Reporting limits unless otherwise stated: water samples I ug/L; vapor samples 0.5 ug/L; solid and sludge samples 5 ug/kg; wipes 0.2ug/wipe <br />ND means not detected above the reporting limit; N/A means analyte not applicable to this analysis <br />(b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-buumone; (g) 4-methyl-2- <br />penumone or isopropylacetone; (h) lighter than water immiscible sheen is present; (i) liquid sample that contains greater than —5 vol. <br />sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br />chlomethene; (o) dimethylbenzenes. <br />DHS Certification No. 1644 <br />/Edward Hamilton, Lab Director <br />