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Sent By: McCampbell Analytical, Inc.; 1 925 798 4612; Mar-10-03 6:01PM; Page 7/10 <br /> ♦_ <br /> 110 2nd.Avenue Suuai..",n7,Paclac9,CA 94551-55W <br /> Ai McCampbellAnalyticalInc. Tdephune:925-]98.1620 Max:925-i9s-1627 <br /> hit,:nwww.mcca bellxom E-mail:nrein'u�nscan Il.mm <br /> John P.Cummings&Associates Client Project ID: #0303001.00;Liberty Date Sampled: 02/28/03 <br /> Fire UST <br /> P.O. Box 2847 Date Received: 03/03/03 <br /> Fremont,CA 94536-2847 Client Contact: John P Cunmlings Date Extracted: 03/03/03 <br /> Client P.O.: Date Analyzed: 03/04/03 <br /> Volatiles Organics by P&T'and GUMS(Basic Target List)* <br /> Extraction Meda,d: SN'50300, Analytical Maliod: SW8260B Work Order 0103008 <br /> _ Lab ID 0303008-001 A <br /> ChentlD Ll'D WI,W2,EI,E2 <br /> Matrix Soil <br /> Compound Concentration" DF °"t1t01' * `1-416, <br /> ume Compound Concentration DF �mdr <br /> Acetone ND 1.0 50 Benzene ND 1.0 5.0 <br /> Bromobenzene ND 1.0 5.0 BiemochlorOrricthanC NU I 5.0 <br /> Bromodichlommethane ND 1050 Bromofomi ND 10 5.0 <br /> Bromomethane ND 10 SO 2Bu_.tanone( ND 1.0 IU <br /> -_ _ MEK)_ ... <br /> n But•I bamzrnu _ __ ND 1.0 , c 0 sec-Butyl benzene ND 1.0 �� 5.0 <br /> grt Butyl benzene NU 1.0 0 Carbon Disulfide ND Lo 5.0 <br /> Carbon Tetmchlonde ND 1.0 5.0- 'Chlorohenzene ND L0 5.0 <br /> Chloroethane ND 1 U 5.0 2-Chloroethyl Vinyl Ether NU LU 5.0 <br /> Chlorofmm ND 10 _ 50 Chloromethane _ ND I0 5.0 <br /> -._. <br /> 2-Clhlorotoluene `!D � 1 0 5.0 d-Chlorotolucnc ND I U 5.0 <br /> Dibmmnchlommethane _ ND 1.0 _ 5.0 1,2-Dihmmo 3chlompropane ND 1 0 5.0 <br /> 1,2 Cyibromoethene(r,DD) NU LU 5.0 Uibromomethane ND 10 5.0 <br /> 12 Dichlorobenzene ND 1.0 5.0 I,3-Dichlorobenzene r ND 1.0 5.0 <br /> [A-Dichlorobenzene NU 1.0 5.0 IAchlorodiflutrin bane ND 10 5.0_ <br /> 11Dichloroethane ND 1.0 50 1,2-Dichlorocthane(1,2DCA) ND 10 5.0 <br /> 1 1 Dichloroethme _ NU 1.0 5.01 1,2-Dn:hloroethene kD 1 0 5 0 <br /> trans t,2-Dichloroethene ND 1.0 _ 5.0 12 D_ichloropiopane NUL0 5.0 <br /> ] 3 Drehlnmpropanc _ ND 10 5 0 2 2 Dlchloropropane ND 10 { 501 <br /> Ti Dlchlo-propene + NO 1 0 50 us 1,3-D,chlompropene NU 10 SD <br /> - _.. <br /> toms-I,3-Nchlompropene ND 1.0 5.0 LthylbcnU ze c ND I 5A) <br /> _ <br /> ..._.. _ - <br /> llexurn <br /> hlorobuladie ND i 10 5,0- 2-Hexanone ND 1'0 I SD <br /> lodometham(Methyl iodide) ND 10 10 4-Isopropyl toluene a MIRK NU 1.11 1 IND 1,0 50 <br /> Isoprapylbenzene ND 1 0 5,0 4 Methyl 0 pe ( ) x.0 <br /> Melhvlenechloride ND I0 5.n Methyl.tbutyl ethei(MTBE) ND 10 5.0 <br /> Naphthalene - --- - NU I) I A 5.0 n Pn,pyl hen<ene NU 10 5.0- <br /> _ ND N1.0 U 1,1,1,2-l etrachlnrocthane ND I 0 5.0 <br /> 161,2 _2=fclrzchloroethane NU �, 1 0 5.0 Telrachlnroethrne ND 10 5,0 <br /> Toluene - ND LU 5A 123-1 nchlorobenzene ND 1.0 5.0 <br /> ... .. ....... .. _ _. <br /> 14 Trichlorobcnzene NU 1 0 5,0 I I-Trichloroethane NU 1 0 5.o <br /> 11.2-Trichloroethene NU _ 10 5.0 Tnchloroethen� p NU 10 Sp <br /> _.._ <br /> Tnchlomflumomethanc ND 1.0 5.0 l 2,3-Tnchloro ro ane ND _ 1 U 5 U <br /> 1,24"I'rime[h�benzene � ND 10 5.0 13,5-Tnmethylbenu__ne ND 1 0 .50 <br /> Lm lAcmate NU LO 50 Vinyl Chloride ND t U 5.0 <br /> Xvlems ND 1.0 5.0 <br /> Surrogate Recoveries <br /> %SSI: 99.9 %SS2: 114 <br /> %SS3: 91.1 <br /> Comments: <br /> water and vapor samples and all TCI.P&SPLP extracts are reported in pli L,soilisludgeisolid samples in pg'kg, wipe samples in lig/wipe, <br /> producVuilmonaqucous liquid samples in mgiL. <br /> ND means not detected above the reporting limit;N:A means analyte not applicable to this analysis. <br /> h)lighter than water immiscible sheemproduct is present;i)liquid sample that conlnins greater than-2 vol.%sediment;j)sample diluted due to high <br /> organic content. <br /> • DHS Certification No. 1644 _ Angela Rydelius,Lab Manager <br />