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Sent By: McCampbell Analytical, Inc. ; 1 925 798 4612; Mar-10-03 6:02PM; Page 8/10 <br /> 110 god Avenue South,HD7,Pacheco,CA 94553-5560 <br /> McCampbell Analytical Tnc. Telephone:925-798-1620 Fax:925-796-1622 <br /> M :."Irccar bell.com E-mail;nan'(41"ldmpbelUoun <br /> John P.Cummings&Associates Client Project ID: #0303001.00;Liberty Date Sampled: 02/28/03 <br /> Fire UST <br /> P.O.Box 2847 Date Received: 03/03/03 <br /> Fremont,CA 94536-2847 Client Contact: John P Cummings Date Fxlracted: 03/03/03 <br /> Client P.O.: Date Analyzed: 03/04/03 <br /> Volatiles Organics by P&T and GC/MS(Basic Target List)* <br /> Exoacdon Medusa: SW5030B Analytic.]Mnhud: SNV82WB Work Order:0303008 <br /> Lab ID 0303008.002A <br /> Client 1D LFD Pipe then <br /> Matrix Soil <br /> Compound Concentration * DF1,,,;;,� Compound Concentration DF xep:nn�s <br /> " tsr <br /> Acetone ND 1.0 50 Benzene ND to 5.0 <br /> Bromobmzene ND 1.0 50 Bromuchlnromethane ND I.0 5.0 <br /> Bromodichloromethane ND LU 5 U Bromuform ND 1.0 5.6 <br /> Bromomahanc ND LO 5.0 243utannne(MEK) i ND 1.0 10 <br /> n-Butyl benzene _ I ND 1 0 _ 50- sec-Butyl ben ere ND 0 5D <br /> ten-Butyl benzene ND 10 U Carbon Disulfide ND IU- 5.0 <br /> Carbon Tetrachloride ND 10 +0 Chlurubenznne ND L0 _ 5.0 <br /> Chloroethane ND_ 10 <br /> 5-0 2-Chlornethvl Vinyl F.ther ND 10 5.0 <br /> Chloroform f ND 1.0 J-.0.Chloromethane ND 1.0 50 <br /> 2-Chlormoluene " ND _ 1.0 _5 0 4 Chl...toluene ND _ 10 50 <br /> Dibromochloromethanc ND 1.0 -5.0- 1,2-Dibrome 3<hloropropane l_ NU 1 U 5.0 <br /> I,2-Dibrom rethane(EDB) W 1 0 _5 0 Dibrumumethan,e ND 1 0 5.0 <br /> 1,2 Dichlorobenzene _ _ _ ND 1.0 5 0 1,3-Dichlorobenzene _ NO 1 0 5.0 <br /> 4-biehlorobenzene NU 1.0 _ 50 Dichluralrnuoromethm�_e NU LU 50 <br /> 1 I-Dichloroahane ND to 50 i 12 Uichluruelhane(1,2-DCA) ND L0 5.0 <br /> 1 1 Dichloroethene ND I 0S0 cis 12-Dichloiaelhene ND _ 1.0 5.0 <br /> trans 1,2-Dichlornethene ND 1.0 5.0 1,2 Uichluruprupane NO L0 5.0 <br /> 1 3 DichloroQropxne - _ -_ <br /> ND <br /> 10 5 D1 5 <br /> I -Dichloropropene .0 _ <br /> 50 cu-1,3-Dichlompro_pene ND t0 50 <br /> trans-I,3-lhchlor ro ne Nll 1 1,0 5 DHtt�lhenzene ND L0 5.0 <br /> Hexachlombuladiene1__ ND I0 0 2-Hexanone _ ND LU 5.0 <br /> lodomethane(Meth ty iodide) ND _ 1.0 10 4-Isopropyl toluene ND I.0 5.0 <br /> Isaprop)Ibenzene __ __ ND IU 50 4-Mcthyl2peentanone(MIBKj _. NDLU 5.11 <br /> Methylene chloride _ ND 1.0 -5.0 I� Methyl-t-butyl ether(M 1,13L) ND I.0 5.0_ <br /> Naphthalene ND I U 5 0 n-Propyl benzene ND 1 0 5.0 <br /> -_.- <br /> Styrene . NU 10 50 1,1,1,2-Tetrachlonxthane ND 10 „5.0 <br /> 11 2,2-Tctrachloroethxne ND 10 50 letrachloroethcnc ND l.0 5p <br /> Toluene ND 10 50 123-Tnchlorobeniene ND 10 50 <br /> L2,4-Trichlomhemm�e_ ND _ 10 _ SU 1 I 1=fnchlorocthanc ND 10 SU <br /> 1,1,2-Trichloroethane - _ ND 1.0 1 5.0 Trichloroethene _ ND 1.0 5.0 <br /> Trichlorofluoromethane ND It) 50 1,2,3-Trichloropropane ND 1.0 5.0 <br /> 12,4-Tr(methYlbenzenc ND t0 50 1,3,5-Tnmethylbenz_ene ND 10 5.0 <br /> Vmyl Aectatc ND l0 50 'i Vinyl Chloride _-_- ND 1.0 5.0 <br /> X lens ND .0 5 0 1 <br /> Surrogate Recoveries(%) <br /> %SSI: 98.3 %SS2: 116 <br /> %SS3: 88.9 <br /> Comments: <br /> *water and vapor samples and all TCLP&SPIT extracts are reported in pg9.,xoib'sludgwsolid samples in pg/kg, wipe samples in pgiwipe, <br /> producticulmon-aqueous liquid samples in mgr L. <br /> ND means not detecled above the reporting limit]NIA means analyte not applicable to this analysis, <br /> h)lighter than water immiscible shem;pruduct is present:i)liquid sample that contains greaser than-2 vol.%sediment,j)sample diluleel due to high <br /> organic content. <br /> DHS Certification No. 1644 Angela Rydelius,Lab Manager <br />