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Quality Control Results <br /> Client: Hyde Environmental, Inc. Job Number: 720-22819-1 <br /> Matrix Spike/ Method:8270C <br /> Matrix Spike Duplicate Recovery Report-Batch: 720.58557 Preparation:35508 <br /> MS Lab Sample ID: 720-22819-1 Analysis Batch: 720-58779 Instrument ID: Sat 2K2 <br /> Client Matrix: Solid Prep Batch: 720-58557 Lab File ID: c:\satumws\epdalMdata\200 <br /> Dilution: 1.0 Initial Weight/Volume: 30.11 g <br /> Date Analyzed: 09/30/2009 1253 Final Weight/Volume: 1 mL <br /> Date Prepared: 0929/2009 0941 Injection Volume: 1.0 uL <br /> MSD Lab Sample ID: 720-22819-1 Analysis Batch: 720-58779 Instrument ID: Sat 21<2 <br /> Client Matrix: Solid Prep Batch. 720-58557 Lab File ID: c:\saturnm\epdata\data\2009( <br /> Dilution: 1.0 Initial WeighWolume: 30.16 g <br /> Date Analyzed: 09/30/2009 1327 Final Weight/Volume: 1 mL <br /> Date Prepared: 09/29/2009 0941 Injection Volume: 1.0 uL <br /> %Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> Acenaphthylene 80 81 49-120 1 35 <br /> 3-Nitroaniline 87 87 39-103 0 35 <br /> Acenaphthene 70 72 42-90 2 35 <br /> 2,4-Dinitrophenol 24 27 13-122 8 35 <br /> 4-Nitrophenol 65 67 25-147 2 35 <br /> Dibenzofuran 73 77 43-96 5 35 <br /> 2,4-Dindrotoluene 80 80 47-107 1 35 <br /> 2,6-Dinitrotoluene 91 87 55-111 5 35 <br /> Diethyl phthalate 82 75 48-105 9 35 <br /> 4-Chlorophenyl phenyl ether 73 71 44-105 3 35 <br /> Fluorene 69 76 41 -102 10 35 <br /> 4-Nitroaniline 81 78 47-120 3 35 <br /> 2-Methy14.6-dinitrophenol 57 58 19-132 3 35 <br /> N-Nitrosodiphenylamine 75 75 43-107 0 35 <br /> 4-Bromophenyl phenyl ether 64 71 45-96 11 35 <br /> Hexachlorobenzene 70 72 48-99 3 35 <br /> Pentachlorophenol 5o 54 7-132 8 35 <br /> Phenanthrene 68 71 38-107 4 35 <br /> Anthracene 72 68 47-98 6 35 <br /> Di-n-butyl phthalate 64 71 46-112 10 35 <br /> Fluoranthene 71 73 40-113 2 35 <br /> Pyrene 71 70 35-101 1 35 <br /> Butyl benzyl phthalate 63 65 40-106 3 35 <br /> 3.3'-Dichlorobenzidine 56 55 17-96 3 35 <br /> Benzo(a]anthracene 69 67 42-102 4 35 <br /> Bis(2-ethylhexyl)phthalate 71 68 42-102 5 35 <br /> Chrysene 68 66 37-97 3 35 <br /> Di-n-octyl phthalate 69 65 46-94 6 35 <br /> Benzo(b]fluoranthene 76 77 43-100 1 35 <br /> Calculations are performed before rounding to avoid round-off errors in calculated results. <br /> TestAmerica San Francisco Page 84 of 102 10/13/2009 <br />