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Quality Control Results <br /> Client: Hyde Environmental, Inc. Job Number: 720-22819-1 <br /> Matrix Spike/ Method:8270C <br /> Matrix Spike Duplicate Recovery Report-Batch: 720-58557 Preparation:3550B <br /> MS Lab Sample ID. 720-22819-1 Analysis Batch: 720-58779 Instrument ID: Sat 2K2 <br /> Client Matrix: Solid Prep Batch: 720.58557 Lab File ID: cAsatum \epdataWata1200 <br /> Dilution: 1.0 Initial WeightfVolume: 30.11 g <br /> Date Analyzed: 09/30/2009 1253 Final WeightlVolume: 1 mL <br /> Date Prepared: 09/29/2009 0941 Injection Volume: 1.0 uL <br /> MSD Lab Sample ID: 720-22819-1 Analysis Batch: 720-58779 Instrument ID: Sat 2K2 <br /> Client Matrix: Solid Prep Batch: 720-58557 Lab File ID: c:lsatumws\epdataldata12009( <br /> Dilution: 1.0 Initial WelghtiVolume: 30.16 g <br /> Date Analyzed: 09/30/2009 1327 Final Weight/Volume: 1 mL <br /> Date Prepared: 09/29/2009 0941 Injection Volume: 1.0 uL <br /> %Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Dual MSD Dual <br /> Benzo[a]pyrene 77 80 48-95 4 35 <br /> Benzo[k]fluoranthene 69 81 39-88 17 35 <br /> Indeno[1,2,3-od]pyrene 77 83 50-106 7 35 <br /> Benzo[g,h,i]perylene 79 91 43-113 13 35 <br /> Benzoic and 0 0 0-85 NC 35 <br /> Azobenzene 76 76 48-95 1 35 <br /> Dibenz(a,h)anthracene 76 75 49-103 1 35 <br /> Surrogate MS%Rao MSD%Rao Pcceptence Limits <br /> Nltrobenzene-d5 72 81 -- —-- 21 -98 <br /> 2-Fluorobiphenyl 69 74 38-96 <br /> Terphenyl-d14 71 72 32-117 <br /> 2-Fluorophenol 72 80 28-98 <br /> Phenol-05 73 81 23-101 <br /> 2,4,6-Tdbromophenol 79 85 37-114 <br /> Calculations are performed before rounding to avoid round-off errors in calculated results. <br /> TestAmenca San Francisco Page 85 of 102 10/13/2009 <br />