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Mr. Jim Walsh <br /> Jul ,• 0• <br /> ' July 15, 1988 <br /> Page 3 <br /> 1 <br /> 1986, 3rd Edition. Samples to be analyzed for high boiling point hydrocar- <br /> bons (HBPH) or semivolatile organics will be collected by filling 250- <br /> milliliter wide-mouth glass jars with soil cuttings from the auger bucket at <br /> the appropriate sampling intervals . After collection, the glass jars will <br /> be sealed with Teflon-lined lids . <br /> Samples to be analyzed for gasoline/benzene, toluene, and xylene (BTX) will <br /> ' be collected with a 2-inch diameter core soil sampler. Before collection , <br /> the soil sampler will be fitted with a stainless steel liner. Next, the <br /> sampler will be driven into the undisturbed soil beyond the base of the <br /> boring at the appropriate sampling interval using a 10-pound hammer with a <br /> ' 20-inch drop. The sampler will then be retrieved from the boring and the <br /> liner will be removed from the sampler . The liner wi11 be wrapped with <br /> Teflon, capped with polypropylene caps, and placed in a screwtop glass jar. <br /> ' After each use, all soil sampling equipment will be decontaminated by steam- <br /> ing with deionized water . All samples will be labeled during sample <br /> ' collection and chain-of-custody documentation will be initiated. The samples <br /> analyzed on site will be composited based on weight by the state-certified <br /> mobile laboratory personnel . Samples taken from the same depth within each <br /> sample zone will be composited, as illustrated in Table 1 . After composit- <br /> ' ing, the samples will be analyzed by the mobile laboratory for HBPH and <br /> gas/BTX. Some of the samples will be transported to an alternate state- <br /> certified laboratory for analysis of semivolatile organic compounds . <br /> ' Analytical Parameters and Procedures <br /> ' Analytical Parameters <br /> The most likely pond contaminants are oil and diesel in storm-water runoff , <br /> originating from trucks parked throughout the facility. Therefore all <br /> ' samples chosen for analysis will be tested for HBPH as oil and diesel . <br /> Selected samples will also be analyzed for gasoline, BTX, and semivolatile <br /> organic compounds, to confirm or deny their presence. <br /> ' Table 2 presents a summary of the analysis plan for the pond composite <br /> samples . All surface and 3-foot composite samples will be analyzed for HBPH <br /> ' as diesel and oil . The 2-foot composite samples will only be analyzed if <br /> the 3-foot composite sample from the respective sampling zone contains less <br /> than 100 parts per million (ppm) of HBPH . If a 3-foot composite sample <br /> contains greater than 100 ppm of HBPH, 4-foot samples will be collected and <br /> ' a composite sample will be prepared from the respective sampling zone and <br /> analyzed . In addition , surface and 2-foot composite samples from the <br /> northwest corner and the middle row will be analyzed for gasoline/BTX and <br /> ' semivolatile organic compounds . <br /> Drainage ditch samples collected at 2 feet below the surface will be <br /> analyzed for HBPH. If a 2-foot sample contains less than 100 ppm of HBPH , <br /> ' the surface sample from that location will be analyzed. If a 2-foot sample <br /> contains greater than 100 ppm of HBPH , the surface sample will not be <br />