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Report Number: 81509 <br /> QC Report : Matrix Spike/Matrix Spike Duplicate Date : 06/12/2012 <br /> Project Name : Tesoro Stockton Terminal <br /> Project Number : 185702499.200.0010 <br /> Duplicate Spiked <br /> Duplicate Spiked Spiked Sample Relative <br /> Spike Spiked Spiked Sample Sample Relative Percent Percent <br /> Spiked Sample Spike Dup. Sample Sample Analysis Date Percent Percent Percent Recov. Diff. <br /> Parameter Sample Value Level Level Value Value Units Method Analyzed Recov. Recov. Diff. Limit Limit <br /> Lead <br /> 81530-01 16 50.0 50.0 67.1 70.4 mg/Kg EPA 6010B 6/12/12 102 108 4.87 75-125 20 <br /> Molybdenum <br /> 81530-01 < 0.25 50.0 50.0 40.5 42.2 mg/Kg EPA 6010B 6/12/12 80.8 84.2 4.10 75-125 20 <br /> Nickel <br /> 81530-01 52 50.0 50.0 104 92.8 mg/Kg EPA 6010B 6/12/12 105 81.8 11.6 75-125 20 <br /> Selenium <br /> 81530-01 < 0.75 50.0 50.0 46.3 47.4 mg/Kg EPA 6010B 6/12/12 91.9 94.2 2.43 75-125 20 <br /> Silver <br /> 81530-01 < 0.25 12.5 12.5 12.1 12.2 mg/Kg EPA 6010B 6/12/12 96.8 97.5 0.782 75-125 20 <br /> Thallium <br /> 81530-01 < 0.75 50.0 50.0 47.0 48.0 mg/Kg EPA 6010B 6/12/12 93.4 95.3 2.04 75-125 20 <br /> Vanadium <br /> 81530-01 46 50.0 50.0 100 88.6 mg/Kg EPA 6010B 6/12/12 108 85.3 12.0 75-125 20 <br /> Zinc <br /> 81530-01 32 50.0 50.0 85.4 81.9 mg/Kg EPA 6010B 6/12/12 107 100 4.18 75-125 20 <br /> TPH as Diesel <br /> 81509-01 13 19.4 19.6 40.2 28.0 mg/Kg M EPA 8015 6/8/12 141 78.2 57.6 60-140 25 <br /> m :30 <br /> - nZ rr <br /> �s T <br /> n ~ <br /> CO N <br /> KIFF ANALYTICAL, LLC z rn <br /> n� rn <br /> 2795 2nd Street, Suite 300 Davis, CA 95618 530-297-4800 �)> <br /> r <br />