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Report Number : 81509 QC Report : Matrix Spike/Matrix Spike Duplicate Date : 06/12/2012 Project Name : Tesoro Stockton Terminal Project Number : 185702499.200.0010 Duplicate Spiked Duplicate Spiked Spiked Sample Relative Spike Spiked Spiked Sample Sample Relative Percent Percent Spiked Sample Spike Dup. Sample Sample Analysis Date Percent Percent Percent Recov. Diff. Parameter Sample Value Level Level Value Value Units Method Analyzed Recov. Recov. Diff. Limit Limit 1,1,1,2-Tetrachloroethane 81501-01 <0.0050 0.0395 0.0384 0.0444 0.0424 mg/Kg EPA 82608 6/7/12 112 110 1.62 70.0-130 25 1,1,1-Trichloroethane 81501-01 <0.0050 0.0395 0.0384 0.0349 0.0334 mg/Kg EPA 82608 6/7/12 88.2 87.0 1.36 70.0-130 25 1,1,2,2-Tetrachloroethane 81501-01 <0.0050 0.0395 0.0384 0.0386 0.0363 mg/Kg EPA 82608 6/7/12 97.6 94.6 3.06 60.7-133 25 1,1,2-Trichloroethane 81501-01 <0.0050 0.0395 0.0384 0.0352 0.0336 mg/Kg EPA 8260B 6/7/12 89.1 87.6 1.64 70.0-130 25 1,1-Dichloroethane 81501-01 <0.0050 0.0395 0.0384 0.0346 0.0333 mg/Kg EPA 8260B 6/7/12 87.6 86.6 1.09 66.1-120 25 1,1-Dichloroethene 81501-01 <0.0050 0.0395 0.0384 0.0346 0.0321 mg/Kg EPA 82608 6/7/12 87.5 83.6 4.56 65.9-122 25 1,1-Dichloropropene 81501-01 <0.0050 0.0395 0.0384 0.0348 0.0333 mg/Kg EPA 82608 6/7/12 88.0 86.7 1.49 70.0-130 25 1,2,3-Trichlorobenzene 81501-01 <0.0050 0.0395 0.0384 0.0277 0.0258 mg/Kg EPA 82608 6/7/12 70.2 67.2 4.32 70.0-130 25 1,2,3-Trichloropropane 81501-01 <0.0050 0.0395 0.0384 0.0370 0.0351 mg/Kg EPA 8260B 6/7/12 93.6 91.4 2.40 70.0-130 25 1,2,4-Trichlorobenzene 81501-01 <0.0050 0.0395 0.0384 0.0317 0.0302 mg/Kg EPA 8260B 6/7/12 80.3 78.8 1.96 70.0-130 25 cn LTi cD -=Z o f>C , �► ry W CO ,0 . KIFF ANALYTICAL, LLC o Z 2795 2nd Street, Suite 300 Davis, CA 95618 530-297-4800 10o r D