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Report Number : 81611 QC Report : Laboratory Control Sample (LCS) Date : 06/19/2012 Project Name : Tesoro Stockton Terminal Project Number : 185702499.200.0007 LCS LCS Percent Spike Analysis Date Percent Recov. Parameter Level Units Method Analyzed Recov. Limit 1,1,1-Trichloroethane 0.0374 mg/Kg EPA 8260B 6/18/12 85.8 70.0-130 1,1,2,2-Tetrachloroethane 0.0374 mg/Kg EPA 8260B 6/18/12 88.9 60.7-133 1,1,2-Trichloroethane 0.0374 mg/Kg EPA 8260B 6/18/12 81.9 70.0-130 1,1-Dichloroethane 0.0374 mg/Kg EPA 8260B 6/18/12 82.8 66.1-120 1,1-Dichloroethene 0.0374 mg/Kg EPA 8260B 6/18/12 82.0 65.9-122 1,1-Dichloropropene 0.0374 mg/Kg EPA 8260B 6/18/12 84.8 70.0-130 1,2,3-Trichlorobenzene 0.0374 mg/Kg EPA 8260B 6/18/12 74.6 70.0-130 1,2,3-Trichloropropane 0.0374 mg/Kg EPA 8260B 6/18/12 85.1 70.0-130 1,2,4-Trichlorobenzene 0.0374 mg/Kg EPA 8260B 6/18/12 89.2 70.0-130 1,2,4-Trimethylbenzene 0.0374 mg/Kg EPA 8260B 6/18/12 87.5 70.0-130 1,2-Dibromoethane 0.0374 mg/Kg EPA 8260B 6/18/12 84.4 67.2-121 1,2-Dichlorobenzene 0.0374 mg/Kg EPA 8260B 6/18/12 91.5 56.3-123 1,2-Dichloroethane 0.0374 mg/Kg EPA 8260B 6/18/12 84.3 64.0-124 1,2-Dichloropropane 0.0374 mg/Kg EPA 82608 6/18/12 77.7 66.6-120 1,2-dibromo-3-chloropropane 0.0374 mg/Kg EPA 8260B 6/18/12 94.6 59.4-138 1,3,5-Trimethylbenzene 0.0374 mg/Kg EPA 8260B 6/18/12 88.6 70.0-130 1,3-Dichlorobenzene 0.0374 mg/Kg EPA 8260B 6/18/12 91.0 52.5-132 1,3-Dichloropropane 0.0374 mg/Kg EPA 8260B 6/18/12 79.9 70.0-130 1,4-Dichlorobenzene 0.0374 mg/Kg EPA 8260B 6/18/12 92.6 57.0-123 2+4-Chlorotoluene 0.0749 mg/Kg EPA 8260B 6/18/12 92.7 70.0-130 2,2-Dichloropropane 0.0374 mg/Kg EPA 8260B 6/18/12 78.0 70.0-130 Benzene 0.0374 mg/Kg EPA 8260B 6/18/12 84.7 67.9-120 n< ' Bromobenzene 0.0374 mg/Kg EPA 8260B 6/18/12 98.3 70.0-130 ; T Z rel N W 0 N � N RZ O Cn M KIFF ANALYTICAL, LLC ZD 2795 2nd Street, Suite 300 Davis, CA 95618 530-297-4800 r