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Report Number : 81611 QC Report : Laboratory Control Sample (LCS) Date : 06/19/2012 Project Name : Tesoro Stockton Terminal Project Number : 185702499.200.0007 LCS LCS Percent Spike Analysis Date Percent Recov. Parameter Level Units Method Analyzed Recov. Limit Bromochloromethane 0.0374 mg/Kg EPA 8260B 6/18/12 86.0 70.0-130 Bromodichloromethane 0.0374 mg/Kg EPA 8260B 6/18/12 89.9 70.0-130 Bromoform 0.0374 mg/Kg EPA 8260B 6/18/12 130 58.2-146 Bromomethane 0.187 mg/Kg EPA 8260B 6/18/12 83.0 45.5-139 Carbon Tetrachloride 0.0374 mg/Kg EPA 8260B 6/18/12 93.4 70.0-130 Chlorobenzene 0.0374 mg/Kg EPA 8260B 6/18/12 92.5 63.4-122 Chloroethane 0.0374 mg/Kg EPA 8260B 6/18/12 87.1 70.0-130 Chloroform 0.0374 mg/Kg EPA 8260B 6/18/12 85.8 67.4-121 Chloromethane 0.0374 mg/Kg EPA 8260B 6/18/12 100 47.9-127 Dibromochloromethane 0.0374 mg/Kg EPA 8260B 6/18/12 103 70.0-130 Dibromomethane 0.0374 mg/Kg EPA 8260B 6/18/12 97.1 70.0-130 Dichlorodifluoromethane 0.0374 mg/Kg EPA 8260B 6/18/12 67.0 40.5-144 Ethylbenzene 0.0374 mg/Kg EPA 8260B 6/18/12 95.0 65.5-127 Hexachlorobutadiene 0.0374 mg/Kg EPA 8260B 6/18/12 97.1 70.0-130 Isopropyl benzene 0.0374 mg/Kg EPA 8260B 6/18/12 94.4 70.0-130 rn Methylene Chloride 0.0374 mg/Kg EPA 8260B 6/18/12 77.1 70.0-130i7- rn Naphthalene 0.0374 mg/Kg EPA 8260B 6/18/12 78.5 70.0-130 < "� O-Xylene 0.0374 mg/Kg EPA 8260B 6/18/12 93.1 62.3-124 O P + M Xylene 0.0374 mg/Kg EPA 8260B 6/18/12 91.3 62.5-124 n � Styrene 0.0374 mg/Kg EPA 8260B 6/18/12 88.4 70.0-130 0 N Tetrachloroethene 0.0374 mg/Kg EPA 8260B 6/18/12 94.3 64.7-122 M 0 rn Toluene 0.0374 mg/Kg EPA 8260B 6/18/12 85.3 65.7-120 n m Trichloroethene 0.0374 mg/Kg EPA 82608 6/18/12 85.6 63.9-121 4 r N N O N KIFF ANALYTICAL, LLC 2795 2nd Street, Suite 300 Davis, CA 95618 530-297-4800