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/ McCampbell Analytical, Inc. 1574 Willow Pass Road,Pittsburg,CA 94565-1701 <br /> 5 Web:www.mccempbeii.com E-mail:main(amcwmpbell.com <br /> "When Ouality Counts" Tele hone:877Q52-9262 Fax:925-252-9269 <br /> QC SUMMARY REPORT FOR SM5520E/F <br /> W.O.Sample Matrix: Soil QC Matrix: Soil BatchlD: 37564 WorkOrder 0808447 <br /> EPA Method SM5520EIF Extraction SM5520EIF Spiked Sample ID: 0808447-001 <br /> Analyte Sample Spiked MS MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria(%) <br /> mg/Kg mg/Kg %Rec. %Rec. %RPD %Rec. %Rec. %RPD I MSI MSD RPD I LCS/LCSD I RPD <br /> POO 81 1000 109 1 106 2.36 93.8 98 4.36 170- 130 1 30 1 70- 130 1 30 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: <br /> NONE <br /> BATCH 37564 SUMMARY <br /> Lab ID Date Sampled Date Extracted Dale Analyzed Lab ID Date Sampled Date Extracted Date Analyzed <br /> 0808447-OOIA 08/13/08 7:45 AM 08/15/08 O9/l8/08 11:55 AM <br /> MS=MaWx Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate;RPD=Relative Percent Deviation. <br /> %Recovery=100'(MSSample)/(Amount Spiked);RPD=100'(MS- MSD)/((MS+MSD)/2). <br /> MS/MSD spike recoveries and I or%RPD may fall outside of laboratory acceptance criteria due to one or mora of the following reasons:a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. <br /> N/A=not enough sample to perform matrix spike and matrix spike duplicate. <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. <br /> DHS ELAP Certification 1644 J2— QA/QC Officer <br />