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34 <br /> 54701 <br /> McCampbellAnalytical, Inc. 5srw.mcowPassRoad,Po-mail:min@m=mpbell.com <br /> E-mail:rvaivCrt mccampbell.com <br /> "When Ouality Counts" Telephone 877-252-9262 Fax:925-252-9269 <br /> QC SUMMARY REPORT FOR SW8015C <br /> W.O.Sample Matrix: Soil QC Matrix: Soil BatchlD: 37577 WorkOrder: 0808447 <br /> EPA Method SW8015C Extraction SW3550C Spiked Sample ID: NIA <br /> Sample Spiked I MS I MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria(°/) <br /> Analyte <br /> mg/Kg mg/Kg %Rec. %Rec. %RPD %Rec. %Rec. %RPD MS I MSD RPD LCS/LCSD RPD <br /> TPR-Diesel(CIO-C23) N/A 20 N/A N/A N/A 96.6 99.9 3.10 N/A N/A 70- 130 30 <br /> %SS: N/A 50 N/A I N/A N/A 105 108 2.99 N/A N/A 70- 130 30 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: <br /> NONE <br /> BATCH 37577 SUMMARY <br /> Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date Extracted Date Analyzed <br /> 0808447-OOIA 08/13/08 7:45 AM 08/15/08 08/15/08 11:29 PM <br /> MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate;RPD=Relative Percent Deviation. <br /> %Recovery=100'(MS-Sample)/(Amount Spiked);RPD=100•(MS- MSD)I((MS+MSD)12). <br /> MS/MSO spike recoveries and/or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons:a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes,with the spike recovery. <br /> N/A=not enough sample to perform matrix spike and matrix spike duplicate. <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. <br /> t/^ <br /> DHS ELAP Certification 1644 ueQA/QC Officer <br />