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• i <br /> McCamabell Analytical, Inc. 1534 Willow Pcs Road,Pittsburg,CA 94565-1701 <br /> Wdx www.maampbcll.mm C+unl:mainCamoampbe8.can <br /> "When Oualim C.MP Tel hone 977-252-9262 Pax:925-252-9269 <br /> QC SUMMARY REPORT FOR SW8015C <br /> W.O.Sample Mallix: Soil OC Matrix: Soil WorkOrder 0807078 <br /> EPA Method SW8075C Extraction SW3550C BatchlD: 36685 Spiked Sample ID: 0807046-002A <br /> Analyte Semple Spiked I MSc%"Rec. <br /> D MS4dSD LCS LCSD LCSLCSD Acceptance Criteria(%) <br /> mglKg mgMg %Re %RPD %Rec. %Rec. %RPD MS/MSD RPD LCS/LCSD RPD <br /> TPH-Diesel(CI O-C23) 4.0 20 98.4 96.9 1.24 100 102 1.55 70- 130 30 70- 130 30 <br /> °iZs 107 50 117 118 0.336 109 100 8.31 70-130 30 70- 130 1 30 <br /> All large(compounds in the Mclhod Blank of this extraction batch were ND Iess than the method RL with the following exceptions: <br /> NONE <br /> BATCH 36685 SUMMARY <br /> Lab ID Date Sampled Dale Extracted Dale Analyzed Lab ID Dale Sampled Date Extracted Date Analyzed <br /> 0807078-ODIA 06/30/08 11:00 AM 07/02/08 07/07/08 10:26 AM 0807078-002A 06/30/08 11:00 AM 07/02/08 07/03/08 6:47 PM <br /> 0807078-003A 06/30/08 11:00 AM 07/02/08 07/03/08 5:38 PM 0807078-004A 06/30/08 11:00 AM 07/02/08 07/04/08 12:29 AM <br /> 0807078-005A 06/30/08 11:00 AM 07/02/08 07/03/08 10:12 PM 0807078-006A 06/30/09 11:00 AM 07102/08 07/03/08 9:03 PM <br /> Me=Metric Spike;MSD=Matrix Spike Duplicate;LCS-Laboratory Control Semple;LCSD=Laboratory Control Semple Duplicate;RPD=Relative Percent Deviation. <br /> %Remvery=t00'(MSSomple)I(Amount Spiked);RPD=100-(MS- MSD)I RMS-MSD)12). <br /> MS/MSD spike recoveries and/or%RPD my fall outside of laboratory acceplanm omens due to one or more of the(allowing reasons:e)the sample is inhomogenous AND <br /> contains significant mncenuaboms of analyte relative In Ne amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. <br /> NIA=not enough sample to perform matrix spike and mains spike dupri®te. <br /> NR=analyte concentration in sample exceeds spike mount for soil matrix or exceeds 2x spike amount far waler matrix or sample diluted due to high matrix or analyte content- <br /> DHS ELAP Certification 1644 ,I QA/QC Officer <br />