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1 <br /> McCampbell Analytical, Inc. 1534Wi11owPossconn Pittsburg,CA 94565-1701 <br /> Web:xwwmme!877-.wm G-moil:nw25�252-9269dLcmn <br /> 1 "When Oualiry Counts" Telephone!R7]-252-9262 Fss:93.252-9269 <br /> QC SUMMARY REPORT FOR SM5520E/F <br /> W.O.Sample Matrix: Soil OC Matrix: Sail WorkOrder 0807078 <br /> EPA Method SM5520EIF Extraction SM5520EIF BatchlD: 36611 Spiked Sample ID: 0806812-OOIA <br /> Analyte Sample Spiked I MS I MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria(%) <br /> mg/Kg mg/Kg 1%Rec.I%Rec.I %RPD I%Rec. %Rec. %RPO MS/MSD RPD LCS/LCSD RPD <br /> POO 690 1000 IIS 111 2.24 106 103 3.37 70- 130 30 70- 130 30 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: <br /> NONE <br /> BATCH 36611 SUMMARY <br /> Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Dale Extracted Date Analyzed <br /> 0807078-OOIA 06/30/08 11 DO AM 07/02/08 07/07/08 2:21 PM 0807078-002A 06/30/08 11:00 AM 07/02/08 07/07/08 2:26 PM <br /> 0807078-003A 06/30/08 11:00 AM 07/02/08 07/07/08 2:31 PM 0807078-004A 06/30/08 11:00 AM 07/02/08 07/07/08 2:36 PM <br /> 0807078-005A 06/30/08 11:00 AM 07/02/08 07/07/OA 2:41 PM11 0807078-006A 06/30/08 11:00 AM 07/02/08 07/07/08 2:46 PM <br /> MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Semple;LCSD=Laboratory Control Sample Duplicate;RPD=Relative Percent Deviation. <br /> %Recovery=100'(MSSample)/(Amount Spiker);RPD=100•(MS- MSD)/((MS-MSD)/2). <br /> MS!MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance altens due to one or more of the following reasons:a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. <br /> N/A=not enough sample to perform mark spike and matrix spike duplicate. <br /> NR=analyle concentration In sample exceads spike amount for soil matrix or exceeds 2r spike amount far water maldx or sample diluted due to high matrix or analyte content. <br /> DHS FLAP Certification 1644 JjP— QA/QC Officer <br />