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1534 Willow Pass RoAd,Pittsburg,CA 94565-1701 <br /> McCampbell Anayticol, Inc. Iol11,re eWpbone (877)25.92621Fax:(925)252-9269 <br /> "When vualiti.Counts" hrtp-- -ww-Mccampbell.cum r 1:-mmil-main<P.mcc=pbdI-cam <br /> Quality Control Report <br /> Client: Ponder Environmental Services Workorder: 1701D08 <br /> Date Prepared: 1130/17 BatchID: 133350 <br /> Date Analyzed: 1/30/17-2/1/17 Extraction Method: SW5030B <br /> Instrument: GC10 Analytical Method: SW8260B <br /> Matrix: Soil Unit: mg/kg <br /> Project: 17-16039;Pacific Ethanol Spill Sample ill: MB/LCS-133350 <br /> 1701 C84-001 AMSIMSD <br /> QC Summary Report for SW8260B <br /> Analyte MB LCS RL SPK MB SS LCS LCS <br /> Rosult Result Val DREG %REC Limits <br /> 1,1-Dichloropropene NO 0.0050 - - <br /> cis-1,3-Dichloropropene NO - 0.0050 - - <br /> trans-1,3-Dichloropropene NO - 0.0050 - - - - <br /> Diisopropyl ether(DIPS) NO 0.0501 0.0050 0.050 - 100 52-129 <br /> Ethylbenzene NO - 0.0050 - - - - <br /> Ethyl tert-butyl elher(ETBE) NO 0,0524 0.0050 0.050 - 105 53-125 <br /> Freon 313 NO - 0.0050 - - - - <br /> Hexachlorobutadiene NO - 0.0050 - - - - <br /> Hexachloroethane NO - 0.0050 - - - - <br /> 2-Hexanone NO - 0.0050 - - - <br /> Isopropylbenzene NO - 0.0050 - - - - <br /> 4-Isopropyl toluene NO - 0.0050 - - - - <br /> Methyl-t-butyl ether(MTBE) NO 0.0523 0.0050 0.050 - 105 58-122 <br /> Methylene chloride NO - 0.0050 - - - <br /> 4-Methyl-2-pentanone(MIRK) NO - 0.0050 - - - <br /> Naphthalene NO 0.0050 - - - - <br /> n-Propyl benzene NO 0.0050 - - - - <br /> Styrene NO - 0.0450 - - - - <br /> 1,1,1,2-Tetrachloroethane NO - 0.0050 - - - - <br /> 1,1,2,2-Tetrachloroethane NO - 0.0050 - - - - <br /> Tetrachloroethene NO - 0.0050 - - <br /> Toluene ND 0.0557 0.0050 0.050 - 1l1 76-130 <br /> 1,2,3-Trichlorobenzene NO - 0.0050 - - - - <br /> 1,2,4-Trichlorobenzene NO - 0-0050 - - - <br /> 11,1-Trichloroethane NO - 0-0050 - - - <br /> 1,1,2-Trichloroethane NO - 0.0050 - - - <br /> Trlchloroethene NO 0.0519 0.0050 0,050 - 104 72-132 <br /> Trichlorofluoromethane NO - 0.0050 - - - - <br /> 1,2,3-Trichloropropane ND - 0.0050 - - - <br /> 1,2,4-Tdmethyl benzene NO - 0.0050 - - - - <br /> 1,3,5-Trimethylbenzene NO _ 0,0050 <br /> Vinyl Chloride NO - 0.0050 - - - - <br /> Xylenes,Total NO 0.0050 - - - <br /> (Cont.) <br /> NE,LAP 40330REI AP `' QA/QC QfFcer <br /> Page 38 of 69 <br />