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w Pass6 <br /> McCam bell Anal tical Inc. 153t!Tctu hww,(8 7)25-926rg,CA 94565.17-1 <br /> � Ton Free'['clephrnir•{R77}257-92G2?Fax:(725)252-9259 <br /> "� h :#w- w.mccam 6cIl.coin?E-mail;maiux?mccam bc%com <br /> "When�uulirs'Cuurrrs �' P P <br /> Quality Control Report <br /> Client: Ponder Environmental Services WorkOrder- 1701D08 <br /> Date Prepared: 1/30117 BatchID: 133350 <br /> Date Analyzed; 1/30/17-2/1/17 Extraction Method: SW5030B <br /> Instrument: GC10 Analytical Method: SW8260B <br /> Matrix: Sail Unit: mg/kg <br /> Project: 17-16039;Pacific Ethanol Spill Sample ID: MBILCS-133350 <br /> 1701 C84-001 AMSIMSD <br /> QC Suntrn:lty Rel)ort for SW8260B <br /> Analyte M8 LCS RL SP1{ MB SS LCS LCS <br /> Result Result Val %REC °IoREC Limits <br /> Surrogate Recovery <br /> Dibromofluoromethane 0.1311 0.733 0.12 105 106 70-130 <br /> Toluene-d8 0.1496 0.151 0.12 120 121 70-130 <br /> 4-BFB 0.01462 0.0152 U12 117 122 70-130 <br /> Benzene-d6 0.1054 0.1 D8 0.10 105 108 60-140 <br /> Ethylbenzene-d10 0.1231 0.126 0.10 123 126 60-140 <br /> 1,2-DCB-d4 0.09669 0.0976 0.10 97 98 60-140 <br /> Analyte MS MSD SPK SPKRef MS MSD MSIMSD RPD RPD <br /> Result Result Val Val °IoREC °IoREC Limits Limit <br /> tent-Amyl methyl ether(TAME) 0.0414 0.0485 0.050 NO 83 97 53-116 9.02 20 <br /> Benzene 0.0380 0.0473 0.050 NO 76 95 63-137 15.0 20 <br /> t-Butyl alcohol(TBA) 0.198 0.248 0.20 NO 99 124 41-135 4.32 20 <br /> Chlorobenzene 0.0369 0.0459 0.050 ND 74,F1 92 77-121 17.8 20 <br /> 1,2-Dibromoethane(EDB) 0.0447 0.0517 0.050 NO 89 103 67-119 13.7 20 <br /> 1,2-Dichloroethane(1,2-DCA) 0.0420 0,0518 0.050 ND 84 103 58-135 14.2 20 <br /> 1,1-Dichloroethene 0.0363 0.9459 0.050 NO 73 92 42-145 12.3 20 <br /> Diisopropyl ether(DIPS) 0.0387 0.0486 0.050 ND 77 97 52-129 14.6 20 <br /> Ethyl tert-butyl ether(ETBE) 0.0422 0.0511 U50 NO 84 102 53-125 11 A 20 <br /> Methyl-t-butyl ether[MTBE] 0.0462_ 0,0534 0.050 NO 92 107 58-122 7.42 20 <br /> Toluene 0.0579 0.0704 0.050 0.02054 75,F1 100 76-130 16.2 20 <br /> Trichloroethene 0-0357 0.0451 0.05- ND 71,F1 90 72-132 15.9 20 <br /> Surrogate Recovery <br /> Dibromofluoromethane 0.134 0.136 0.12 107 109 70-130 1.27 20 <br /> Toluene-d8 0.148 0.150 0.12 118 120 70-130 2.39 20 <br /> 4-BFB 0.0179 0.0182 0.012 143 146,F3 70-130 6.86 20 <br /> Benzene-d6 0.0840 0.103 0.10 84 103 60-140 13.4 20 <br /> Ethylbenzene-d10 0.0806 0.105 MID 81 106 60-140 24.3,F1 20 <br /> 1,2-DCB-d4 0.0807 0.113 _ 0.10 81 113 60-140 32.5.F1 20 <br /> (Cont.) <br /> NELAP 403301.ELAP ` QA/QC Officer <br /> Page 39 of 69 <br />