Laserfiche WebLink
9.0QUALTMy ASSURANCE PLAN <br /> 3 , 1 General Sample collection and Hg dlina procedures <br /> Proper collection and handling are essential to ensure the <br /> quality of a sample. Each sample will be collected in a suitable <br /> container, preserved correctly for the intended analyses, and <br /> stored prior to analysis for no longer than the maximum allowable <br /> holding time. Details on the procedure for collection and han- <br /> dling of soil samples to be used on this project can be found in <br /> Section 1 . 0 (Methods) . <br /> ale Identifica*�or and Chain-of-Cuetody Procedures <br /> Sample identification and chain-of-custody procedures ensure <br /> sample integrity and document sample possession from the time of <br /> collection to its ultimate disposal. Each sample container <br /> submitted analysis will have a label affixed to identify the job <br /> number, date, and time of sample collection, and a sample number <br /> unique to that sample. This information, in addition to a de- <br /> scription of the sanple, field measurements made, sampling <br /> methodology, names of on-site personnel , and any other pertinent <br /> field observations will be recorded on the borehole log in the <br /> field records. All samples will be analyzed by a State-certified <br /> laboratory. <br /> A chain-of-custody form will be used to record possession of the <br /> sample from time of collection to ifs arrival at the laboratory. <br /> When the samples are shipped, the person in custody of them will <br /> relinquish the samples by signing the chain-of-custody form and <br /> noting the time. The sample-control officer at the laboratory <br /> will verify sample integrity and confirm that it was collected in <br /> the proper container, preserved correctly, and that there is and <br /> adequate volume for analysis. <br /> If these conditions are met, the sample will be assigned a unique <br /> log number for identification throughout analysis and reporting. <br /> The log number will be recorded on the chain-of-custody form and <br /> in the legally-required log book maintained by the laboratory in <br /> the laboratory. The sample description, date received, client' s <br /> name and any other relevant information will also be recorded. <br /> 1 . 2 Analytical Quality Assurance <br /> In addition to routine calibration of the analytical instruments <br /> with standards and blank, the analyst is required to run dupli- <br /> cates and spikes on 10 percent of the analyses to insure an added <br /> measure of precision and accuracy. Accuracy is also verified <br /> through the following: <br /> 1 . U. S. Environmental Protection Agency (EPA) and State cer- <br /> tification programs. <br /> Page! 2 <br />