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07/21/2004 14:23 2095720 GEO PAGE 07/15 <br />GeoAnaiyticai Laboratories, Inc. <br />1405 Kansas Avenue Modesto, CA 95351 Phone (209) 572-0900 Fax (209) 572-0916 <br />Report# Q184-08 <br />CERTIFICATE OF ANALYSIS <br />Date: 7/12/04 <br />Thorpe Oil <br />Date Itec'd: 7/02/04 <br />PO Box 357 <br />Lodi <br />Project: 601 E. Main St. - Stockton <br />Date Started: 7/08/04 <br />CA <br />95241 <br />Date Campleted:7/08/04 <br />PD# <br />Date Sampled: 7/02/04 <br />Sample ID: TK -2 <br />Time: <br />Lab ID: +200949 <br />Sampler: R. Bombaywala (Geo) <br />Method <br />RL <br />Anal to <br />ResuIts Units <br />8260B <br />5.0 <br />Benzene <br />5.0 <br />Toluene <br />ND <br />5.0 <br />Ethyl Benzene <br />5-0 <br />Total Xylenes <br />8.6 <br />10 <br />Methyl tert-butyl ether (MTBE) <br />31 <br />ND <br />400 <br />Ethanol <br />200 <br />tert-Butanol <br />ND <br />D <br />10 <br />di -Isopropyl ether (DiPE) <br />N D <br />ND <br />10 <br />Ethyl tart -butyl ether (ETRE) <br />10 <br />tert-Amyl methyl ether {TAME) <br />lD <br />Surrogate Aznnt Spiked <br />1,2-Dichloroethane-d, 20 <br />Amnt ilea <br />QC Limit 1! <br />�O R57 <br />2-Bromo-l-chloropropane 20 <br />Oery <br />31 4 <br />26.1 <br />4-13rornotluorobenzene 20 <br />130.5 63-139 <br />27.6 138.0 64-136 <br />�al <br />Matt Pagecr�-��,� <br />S <br />Chemist <br />Certification # 1157 <br />Donna Keller <br />Laboratory Director <br />