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67/21/2104 14:23 <br />2095726916 GEG <br />Amnt Rec. e y QC Limit ' '. <br />/A Recovere-d, <br />2-Brorno-l-chloropropane <br />400 <br />402 100.5 66-133 <br />510 <br />4-Bramofluorobenzene <br />400 <br />PAGE 88/15 <br />. <br />GeoAna ytical Laboratories, Inc. <br />1405 Kansas Avenue Modesto, CA 95351 Phone (249) 572-0900 Fax (209) 572-0916 <br />Report# Q184-08 <br />CERTIFICATE OF ANALYSIS <br />Laboratory Director <br />Date: <br />7/12/04 <br />Thorpe Oil <br />PO Box 357 <br />Date Rec'da <br />7/02/04 <br />Lodi <br />Project: 601 E. Main St. - Stockton <br />Date Started: <br />7/08/04 <br />CA <br />95241 <br />Date Completed- <br />7/09/04 <br />PO# <br />Date Sampled: <br />7/02/04 <br />Sample ID: Hot Pile <br />Time: <br />Lab ID: Q200950 <br />Sampler: R. Bornbaywala (Geo) <br />Method <br />RL <br />Anal to <br />82608 <br />100 <br />Benzene <br />Results <br />Units <br />100 <br />Toluene <br />106 <br />tig/Kg <br />1001010 <br />Ethyl Benzene <br />100 <br />'Total Xylenes <br />953 <br />2005450 <br />Methyl vert -butyl ether (MME) <br />8000 <br />Ethanol <br />ND <br />9000ND <br />tent -Butanol <br />200 <br />di -Isopropyl ether (DIpE) <br />NDND <br />2M <br />Ethyl tert-butyl ether (E?BE) <br />ND <br />200 <br />tert-Amyl rnethyl ether (TAYLE) <br />NO <br />" OC Criteria not Met due to high level of analyte <br />concentration <br />Matt Page <br />Chemist <br />Surrogate <br />1,2-Dichloroethan <br />Amnt Spiked <br />400 <br />Amnt Rec. e y QC Limit ' '. <br />/A Recovere-d, <br />2-Brorno-l-chloropropane <br />400 <br />402 100.5 66-133 <br />510 <br />4-Bramofluorobenzene <br />400 <br />127.5 63-139 <br />664'F 166.0 <br />64-136 <br />Certification # 1157 <br />Donna Keller <br />Laboratory Director <br />