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GeoAnalytical Laboratories, Inc. <br />1405 Kansas Avenue Modesto, CA 95351 Phone (209) 572-0900 Fax(209)572-0916 <br />Date: 09/11/07 <br />Report # T71-12801 Project: BJJ Company LLC <br />Date Recd: 08/28,107 <br />Jim Thorpe, Inc. <br />PO Box 357 PO#: <br />Lodi, CA 95241 <br />Volatile Organic Chemistry - Quality Control <br />GeoAnalytical Laboratories, Inc. <br />Reporting Spike Source %REC RPD <br />4nalvte Result Limit Units Level Result %REC Limits RPD Limit Notes <br />Batch T003093 - EPA 5030B <br />Prepared & Analyzed: 09/10/07 <br />Blank (T003093-BLKI) <br />Dibromochloromethane <br />ND <br />5.0 ug/kg <br />Dibromomethane <br />ND <br />5.0 " <br />DichlorodiFluoromethane(FREON 12) <br />ND <br />5.0 " <br />Ethylbenzene <br />ND <br />5.0 " <br />Ethylene dibmmide <br />ND <br />5.0 " <br />Hexachlorobutadiene <br />NO <br />5.0 " <br />Isopropylbenzene(Cumene) <br />ND <br />5.0 " <br />m,p-Xylene <br />ND <br />5.0 " <br />Methyl ten -Butyl Ether (MTBE) <br />ND <br />5.0 " <br />Methylene Chloride <br />ND <br />20.0 " <br />Monochlorobenzene <br />ND <br />5.0 " <br />n-Butylbenzene <br />ND <br />5.0 " <br />n -Propyl Benzene <br />ND <br />5.0 " <br />o -Xylene <br />ND <br />5.0 " <br />p4sopropyholuene <br />NO <br />5.0 " <br />sec-Butylbenzene <br />ND <br />5.0 " <br />Styrene <br />NO <br />5.0 " <br />ten-Butylbenzene <br />ND <br />5.0 " <br />Tetrachloroethylene(PCE) <br />ND <br />5.0 " <br />Toluene <br />ND <br />5.0 " <br />trans-l,2-Dichloroethylene <br />ND <br />5.0 " <br />Trichloroethylene <br />ND <br />5.0 " <br />Trichlorofluoromethane <br />ND <br />5.0 " <br />Trichlorotrifluomethane <br />ND <br />5.0 <br />Vinyl chloride <br />ND <br />5.0 " <br />Surrogate: 1.1-Dichloroethane-d4 16.9 10.00 84 71-132 <br />Surrogate. 2-Bromo-1-Chloropropane 17.1 20.00 86 71-134 <br />Surrogate: 4-Bromuluorobemene 18.4 20.00 92 74-131 <br />Certification # 2585 <br />