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M <br />GeoAnalytical Laboratories, Inc. <br />1405 Kansas Avenue Modesto, CA 95351 Phone(209)572-0900 Fax(209)572-0916 <br />Date: 09/11/07 <br />Report # T7H2801 Project: BJJ Company LLC <br />Date Recd: 08/28/07 <br />Jim Thorpe, Inc. <br />PO Box 357 PO#: <br />Lodi, CA 95241 <br />Volatile Organic Chemistry - Quality Control <br />GeoAnalytical Laboratories, Inc. <br />Reporting Spike Source %RE.0 RPD <br />tnaNte Result Limit Units Level Result %REC Limits RPD Limit Notes <br />Batch T003093- EPA 5030B <br />Prepared & Analyzed: <br />09/10/07 <br />43.8 5.0 ug/kg <br />LCS (T003093 -BSI) <br />ND <br />110 <br />73-144 <br />44.7 5.0 <br />40.00 <br />I,1-Dichlorcethane <br />42.8 <br />5.0 <br />ug/kg 40.00 <br />107 <br />80-120 <br />Benzene <br />43.0 <br />5.0 <br />40.00 <br />107 <br />80-120 <br />Methyl ten -Butyl Ether (MTBE) <br />46.2 <br />5.0 <br />" 40.00 <br />116 <br />80-120 <br />Monochlorobenzene <br />43.4 <br />5.0 <br />40.00 <br />109 <br />80-120 <br />Toluene <br />44.1 <br />5.0 <br />40.00 <br />110 <br />80-120 <br />Trichlomethylcnc <br />44.3 <br />5.0 <br />40.00 <br />111 <br />80.120 <br />Surrogate: 1,2-Dichloroerhaned4 <br />10.0 <br />Source: T71-12801-07 <br />20.00 <br />100 <br />71-131 <br />Surrogate. 2-Bromo-I-Ch1oropropane <br />18.8 <br />40.00 <br />10.00 <br />94 <br />71-134 <br />Surrogate: 4-BromoJluorobemene <br />19.8 <br />ND <br />20.00 <br />99 <br />74-132 <br />Matrix Spike (T003093 -MSI) <br />I,1-Dichloroethane <br />Benzene <br />Methyl Leri -Butyl Ether (MTBE) <br />Monochlorobenzene <br />Toluene <br />Trichloroethylene <br />Surrogate: 1, 2-Dichloroethane-d4 <br />Surrogate: 2-8mmo-1-Chloropropane <br />Surrogate: 4-Bromo/luorobenzene <br />Matrix Spike Dup (T003093-MSDI) <br />I,1-Dichlorcelhane <br />Benzene <br />Methyl tert-Butyl Ether(MTBE) <br />Monochlombenzene <br />Toluene <br />Trichloroethylene <br />Surrogate: 1,2-Dichlorcethane-d4 <br />Surrogate: 2-Broma-1-Chloropropane <br />Surrogate: 4-8romojIuorobenzene <br />Source: T711112801-07 <br />43.8 5.0 ug/kg <br />40.00 <br />ND <br />110 <br />73-144 <br />44.7 5.0 <br />40.00 <br />ND <br />112 <br />80423 <br />46.4 5.0 <br />40.00 <br />ND <br />116 <br />75-139 <br />38.4 5.0 <br />40.00 <br />ND <br />96 <br />59-151 <br />40.9 5.0 <br />40.00 <br />ND <br />102 <br />67-135 <br />44.0 3.0 <br />40.00 <br />ND <br />110 <br />69-143 <br />21.3 <br />20.00 <br />106 <br />71-132 <br />17.5 <br />10.00 <br />87 <br />71-134 <br />10.9 <br />10.00 <br />104 <br />74-132 <br />Source: T71-12801-07 <br />38.6 5.0 ug/kg <br />40.00 <br />ND <br />97 <br />73-144 <br />38.6 5.0 " <br />40.00 <br />ND <br />97 <br />80-123 <br />43.1 5.0 <br />40.00 <br />ND <br />108 <br />75.139 <br />37.6 5.0 <br />40.00 <br />ND <br />94 <br />59-151 <br />38.8 5.0 <br />40.00 <br />ND <br />97 <br />67.135 <br />37.8 5.0 <br />40.00 <br />ND <br />95 <br />69-143 <br />20.9 <br />10.00 <br />105 <br />72-132 <br />20.7 <br />20.00 <br />103 <br />71-134 <br />19.3 <br />20.00 <br />96 <br />74-131 <br />Certification # 2585 <br />13 <br />IS <br />7 <br />2 <br />5 <br />15 <br />18 <br />16 <br />20 <br />19 <br />13 <br />15 <br />