Laserfiche WebLink
�uo5 09;01 209468 433 EHD • PAGE 06 <br /> r <br /> MINIMUM VERIFICATION LABORATORY ANALYSIS <br /> TA 'K TANK TPH-G TPH•D 13TX&E CL HC TOTAL , MTBE AT OXy0EN <br /> [ CONTENTS scar^t PCB <br /> 8013 8015 8020 8010 LOAD 8020 (bfTBE, <br /> 8260 8260 8260 8240 7420 Te DIP 1CAP/ 8270 <br /> 6260 11 �• AES or 8080 <br /> 8260 7gy1 TAML <br /> TAML') AA <br /> 8260 <br /> LEADED GAS X X X <br /> X <br /> UNL GAS X X X <br /> I.ESEI, X X <br /> KEROSENE X X X <br /> UNK FUEL X X X X <br /> X <br /> PROD.OIL X X X <br /> CHLOR. <br /> SOLVENTS X X X <br /> NONCFILOR <br /> SOL'VEN'TS X X X <br /> WASTE% <br /> USED OIL X X X X <br /> X X X <br /> All na ysls methods arc the designated EPA methods described In EPA SW 846,Third Edition. Those methods not found <br /> Inves6 ht SW.846 are <br /> ally noted below, Refer to the "SWRCB LUF'i' Field Manual",Appendix D (B),Table 3.5 on page A20 for minimum detection <br /> specific <br /> limits r motor vehicle fuel (gasoline and diesel). Refer to "Tri-Regional Board Staff Rccommeidatlons for Initial Evaluation and <br /> tion of UST's" for the waste and motor oil minimum doteotion limits. Detection Limits that ram In below the MCL,STLC or <br /> ABa uwIe Limit or the contaminant in question will be accepted,however laboratory shall utilize the most conservative method. <br /> LABORATORY ANALYSES <br /> TPH-G Total Petroleum klydrocarbon,Gasoline,GC/FID(5030)8015 mod or GC/MS 8260OLOGY: <br /> 1PH-D Total Petroleum Hydrocarbon,Diesel,CUPID(3550),8015 mod or GC/MS 8260 <br /> BTX& Benxene,Toluene,Xylcne&Ethyl Benzene,GC/PID 8020 or GUMS 8260 <br /> CL HC Chlorioatcd I lydrocarbon,GC/FISD 8010,GC/MS R24D or 8260 <br /> TOTAL EAD Taal lean AA 7420, AA 7421 or(CP-AES 6010 <br /> OXYGEIIATES MTBE,ETBE,TAME,DIPE,&TBA GC/)4S 8260(Por MTBE screen nolo you may use 8020) <br /> MET ICAP or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption Specttwnetry 7000. Motais: <br /> Cadmium,Chromium 171 and VI,Lead,Zine and Nickel. <br /> PCB Polychlorinated Siphonyb,GC/MS 8270 or 8080 <br /> CC-FID Gas ClatOMMography,Flame Ionization Deiectlon <br /> Method USO Acid digestion <br /> Method 3 40 Soxhlcl sample preparation <br /> Method 3 50 Sonication sample preparutioa,extraction method <br /> Method S 30 Purge low trip sample preparation <br /> QA/QC Quality Assumnce/Qualiry Control <br /> Nola: To avoid false positive detection of benzene,benzene•frev solvents we to be used. Fused capillmy columns ore preferred to Docked columns',a <br /> packed col unin may be used as a'first cut"with"dirty"sampies or once the hydrocarbons have been characterized and proper QA/QC is followed. For <br /> drinking later$wives,EPA recommends that the 500 series for volatile orbanie should be usad inprCA ' <br /> nce to the 600 series because the detection <br /> limit,are I mer and the QA/QC is better. Samples exhibiting any level of heavy metal cootomination may require further analysis.PHS.EHD <br /> recominen Is isolding those sample$until disposal is indicated. <br /> EH 23 046 (Revised 05/09)00) <br /> 5 <br />