Upon reaching TD,drilling fluid is circulated to remove cuttings. Vapor samples are subject to very limited holding times,typically 48
<br /> Selected casing is then run into the borehole and set to the desired hours. Thus,care must taken to avoid delays in submittal of vapor
<br /> depth. Monitoring wells are cased with clean,threaded,factory- samples to the laboratory. In the event the vapor samples cannot be
<br /> perforated and blank casing. The perforated interval consists of slotted submitted to the analytical laboratory on the same day they are
<br /> casing,generally with 0.020-inch-wide by 1.5-inch-long slots,with 42 collected,they are to be temporarily stored in the dry,non-refrigerated,
<br /> slots per foot. Centering devices may be fastened to the casing the packed cooler until the very first opportunity for submittal well within the
<br /> ensure even distribution of fitter material and grout within the borehole required holding time,taking into account the time needed for shipment
<br /> annulus. The well casing is thoroughly washed and/or steam cleaned, to and receipt by the laboratory.
<br /> or may be purchased as pre-cleaned,prior to installation. All
<br /> recoverable drilling fluid and/or cuttings are collected for temporary SOP-10
<br /> storage and disposed of properly pending analytical results. VAPOR SAMPLING:SYRINGE SAMPLING TECHNIQUE
<br /> After setting the casing,sand or gravel filter material is poured into the Prior to vapor sampling,the vacuum system must reach a stabilized air
<br /> annular space to fill from boring bottom to generally 1 foot above the flow(cubic feet per minute)for approximately 15 minutes. Prior to the
<br /> perforated interval. A 1-to 2-foot-thick bentonite plug is set above this actual collection of the vapor sample,the following data is recorded:air
<br /> filter material to prevent grout from infiltrating the filter pack. Either flow,temperature,and pressure at collection ports and gauges.
<br /> neat cement,containing about 5 percent bentonite,or sand-cement
<br /> grout is then tremmied into the annular space from the top of the The sampling equipment consists of a clean, 10occ,gas-tight syringe
<br /> bentonite plug to near surface. A traffic-rated vault is installed around and silicone septa.
<br /> each wellhead for wells located in parking lots or driveways,while steel
<br /> "stovepipes"are usually set over wellheads in landscaped areas. The sampling ports are brass connections,fitted with silicone septa,
<br /> and threaded into a tapped hole in the system piping. Samples are
<br /> After installation,the wells are thoroughly developed to remove residual collected by inserting a clean syringe into the septum and the plunger
<br /> drilling materials from the wellbore,and to improve well performance by actuated several times. Each syringe should be purged of three
<br /> removing fine material from the fitter pack that may pass into the well. syringe volumes before collecting the sample. On the fourth purge,the
<br /> Well development techniques used may include pumping,surging, plunger is extracted slowly until the syringe is filled with a gas sample,
<br /> bailing,swabbing,letting,flushing,and air-lifting. All development then the syringe is withdrawn and the needle immediately plugged with
<br /> water is collected either in drums or tanks for temporary storage,and a silicone stopper. The sample should be placed in a non-refrigerated,
<br /> properly disposed of pending laboratory analytical results. To minimize dry cooler with sufficient packing to eliminate breakage during
<br /> the potential for cross-contamination between wells,all development transport. Cooling samples will cause condensation of moisture,
<br /> equipment is either steam cleaned or properly washed prior to use. thereby distorting laboratory analysis.
<br /> Following development,the well is allowed to stand undisturbed for a
<br /> minimum of 24 hours before its first sampling. For quality control purposes,a duplicate air sample should be collected
<br /> from each port. This sample is put on hold at the laboratory pending
<br /> Initial analysis.
<br /> SOPS
<br /> VAPOR SAMPLING:"TEDLAR"BAG SAMPLING TECHNIQUE Vapor samples are subject to very limited holding times,typically 48
<br /> hours. Thus,care must taken to avoid delays in submittal of vapor
<br /> Prior to vapor sampling,the vacuum system must reach a stabilized air samples to the laboratory. In the event the vapor samples cannot be
<br /> flow(cubic feet per minute)for approximately 15 minutes. Prior to the submitted to the analytical laboratory on the same day they are
<br /> actual collection of the vapor sample,the following data is recorded:air collected,they are to be temporarily stored in the dry,non-refrigerated,
<br /> flow,temperature,and pressure at collection ports and gauges. packed cooler until the very first opportunity for submittal well within the
<br /> required holding time,taking into account the time needed for shipment
<br /> The sampling equipment consists of a"Tedlar'bag(available in 1,3,5, to and receipt by the laboratory.
<br /> and 10 liter sizes),a diaphragm pump,and 1/4-inch-diameter
<br /> polyethylene tubing(approximately 1 foot long). SOP-11
<br /> VAPOR SAMPLING:CANISTER SAMPLING TECHNIQUE
<br /> The sampling ports are brass connections,fitted with a silicone septa,
<br /> and threaded into a tapped hole in the system piping. The sampling Prior to vapor sampling,the vacuum system must reach a stabilized air
<br /> procedure requires one end of the tubing be slipped over the sampling flow(cubic feet per minute)for approximately 15 minutes. Prior to the
<br /> port and the other end over the diaphragm pump to acquire an air-tight actual collection of the vapor sample,the following data is recorded:air
<br /> connection. The sampling pump is purged for 1 minute with the flow,temperature,and pressure at collection ports and gauges.
<br /> extracted vapor to be sampled. Following purging,the discharge of the
<br /> pump Is then diverted through a two-way valve into the"Tedlar'bag, The sampling equipment consists of a sterilized,gas-tight,"Vacu-
<br /> which should be filled to 3/4 of volume capacity. Caution should be Sampler'stainless steel canister,and 1/4-inch-diameter polyethylene
<br /> taken not to overfill the sampling bag. The sample is placed in a non- tubing approximately 2 feet in length.
<br /> refrigerated dry cooler with sufficient packing to eliminated damage
<br /> during transport. Cooling samples will cause condensation of moisture The sampling ports are brass connections fitted with silicone septa and
<br /> within the sample,thereby distorting laboratory analysis. threaded into a tapped hole in the system piping. The sampling
<br /> procedure requires one end of the tubing to be slipped over the
<br /> For quality control purposes,a duplicate vapor sample should be sampling port and the other end over the canister nozzle to acquire an
<br /> collected from each sampling port. This sample is then put on hold at air-tight connection. The actuator on top of the canister Is depressed
<br /> the laboratory pending initial analysis. To ensure quality control and for 10 seconds. At the end of the 10 seconds,the canister is
<br /> minimize the potential for cross-contamination prior to and during disconnected from the tubing and the tubing is disconnected from the
<br /> sampling,the diaphragm pump is thoroughly purged for approximately sampling port. Immediately following the sample collection,complete
<br /> 5 minutes with nitrogen or clean air(i.e.,compressed clean air). A sampling information is recorded on the label on the air sampling
<br /> "blank"sample of the discharged air is captured in a"Tedlar"bag at the canister(e.g.,sample ID,date,time,location,and temperature). The
<br /> end of the purging procedure and may be analyzed to ensure the sample is placed in a non-refrigerated,dry cooler with sufficient
<br /> purging was effective. packing to ensure against damage during transport. Cooling samples
<br /> will cause condensation of any moisture within the air sample,thereby
<br /> To minimize the potential for cross-contamination between air samples, distorting laboratory analysis,
<br /> the polyethylene tubing,if not sample dedicated,is thoroughly cleaned
<br /> and rinsed.
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