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For quality control purposes,a duplicate vapor sample should be <br /> collected from each sampling port. This sample is then put on hold at <br /> the laboratory pending the initial analysis. To minimize the potential for <br /> cross-contamination between vapor samples,the polyethylene tubing,if <br /> not sample dedicated,is thoroughly cleaned and rinsed. <br /> Vapor samples are subject to very limited holding times,typically 48 <br /> hours. Thus,care must taken to avoid delays in submittal of vapor <br /> samples to the laboratory. In the event the vapor samples cannot be <br /> submitted to the analytical laboratory on the same day they are <br /> collected,they are to be temporarily stored in the dry,non-refrigerated, <br /> packed cooler until the very first opportunity for submittal well within the <br /> required holding time,taking into account the time needed for shipment <br /> to and receipt by the laboratory. <br /> SOP-12 <br /> MEASURING LIQUID LEVELS USING WATER LEVEL METER OR <br /> INTERFACE PROBE <br /> Field equipment used for liquid-level gauging typically includes the <br /> measuring instrument(water-level meter or interface probe)and <br /> product bailer(s). The field kit also includes cleaning supplies <br /> (buckets,solution,spray bottles,and deionized water)to be used in <br /> cleaning the equipment between wells. <br /> Prior to measurement,the instrument tip is lowered into the well until It <br /> touches bottom. Using the previously established top-of-casing or top- <br /> of-box(i.e.,wellhead vault)point,the probe cord(or halyard)is marked <br /> and a measuring tape(graduated in hundredths of a foot)is used to <br /> determine the distance between the probe end and the marking on the <br /> cord. This measurement is then recorded on the liquid-level data sheet <br /> as the"Measured Total Depth"of the well. <br /> When necessary in using the interface probe to measure liquid levels, <br /> the probe is first electrically grounded to either the metal stove pipe or <br /> another metal object nearby. When no ground is available, <br /> reproducible measurements can be obtained by clipping the ground <br /> lead to the handle of the interface probe case. <br /> The probe tip is then lowered into the well and submerged in the <br /> groundwater. An oscillating(beeping)tone indicates the probe is in <br /> water. The probe is slowly raised until either the oscillating tone <br /> ceases or becomes a steady tone. In either case,this is the depth-to- <br /> water(DTW)indication and the DTW measurement is made <br /> accordingly. The steady tone indicates floating liquid hydrocarbons <br /> (FLH). In this case,the probe is slowly raised until the steady tone <br /> ceases. This is the depth-to-product(DTP)indication and the DTP <br /> measurement is made accordingly. <br /> The process of lowering and raising the probe must be repeated <br /> several times to ensure accurate measurements. The DTW and DTP <br /> measurements are recorded on the liquid-level data sheet. When FLH <br /> are indicated by the probe's response,a product bailer is lowered <br /> partially through the FLH-water interface to confirm the FLH on the <br /> water surface and as further indication of the FLH thickness, <br /> particularly in cases where the FLH layer is quite thin. This <br /> measurement is recorded on the data sheet as"FLH thickness" <br /> In order to avoid cross-contamination of wells during the liquid-level <br /> measurement process,wells are measured in the order of"clean"to <br /> "dirty"(where such information is available). In addition,all <br /> measurement equipment is cleaned with solution and thoroughly rinsed <br /> with deionized water before use,between measurements in respective <br /> wells,and at the completion of the days use. <br />