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Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 <br /> Job Number: C31148 <br /> Account: ENCOCALA Encon Solutions, Inc. <br /> Project: 1145 S. Aurora Street-Stockton, CA <br /> Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch <br /> OP9141-MS HH309574.D 1 11/27/13 AG 11/27/13 OP9141 GHH 1141 <br /> OP9141-MSD HH309575.D 1 11/27/13 AG 11/27/13 OP9141 GHH1141 <br /> C31149-14 HH309566.D1 11/27/13 AG 11/27/13 OP9141 GHH1141 <br /> The QC reported here applies to the following samples: Method: SW846 8015B M <br /> y <br /> C31148-2, C31148-4, C31148-6, C31148-8, C31148-10, C31148-12 74 <br /> i� <br /> C31149-14 Spike MS MS MSD MSD Limits <br /> CAS No. Compound mg/kg Q mg/kg mg/kg % mg/kg % RPD Rec/RPD <br /> TPH(C10-C28) 2.65 J 97.1 77.2 77 82.7 82 7 39-102/29 <br /> TPH(> C28-C40) ND 97.1 78.1 80 83.9 86 7 42-111/26 <br /> CAS No. Surrogate Recoveries MS MSD C31149-14 Limits <br /> 630-01-3 Hexacosane 91% 92% 92% 37-122% <br /> * = Outside of Control Limits. <br /> No 70 of 80 <br /> 8.a.r-.C::tJTF=S;T <br /> C31148 `...--I- <br />