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Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 <br /> Job Number: C31148 <br /> Account: ENCOCALA Encon Solutions, Inc. <br /> Project: 1145 S. Aurora Street-Stockton, CA <br /> Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch <br /> OP9144-MS GG49063.1) 1 11/27/13 NN 11/27/13 OP9144 GGG1349 <br /> OP9144-MSD GG49064.D 1 11/27/13 NN 11/27/13 OP9144 GGG1349 <br /> C31148-16 GG49062.D 1 11/27/13 NN 11/27/13 OP9144 GGG1349 <br /> The QC reported here applies to the following samples: Method: SW846 8015B M <br /> y <br /> C31148-14, C31148-16 74 <br /> C31148-16 Spike MS MS MSD MSD Limits <br /> CAS No. Compound mg/kg Q mg/kg mg/kg % mg/kg % RPD Rec/RPD <br /> TPH(C10-C28) 2.54 J 99.5 71.5 69 77.5 75 8 39-102/29 <br /> TPH(> C28-C40) ND 99.5 78.7 79 85.9 86 9 42-111/26 <br /> CAS No. Surrogate Recoveries MS MSD C31148-16 Limits <br /> 630-01-3 Hexacosane 80% 86% 88% 37-122% <br /> * = Outside of Control Limits. <br /> No 69 of 80 <br /> 8.a.r-.C::tJTF=S;T <br /> C31148 `...--I- <br />