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Mr. Verrill Norwood -3- <br /> 6 August 1996 <br /> Task 4 - Laboratory Analysis <br /> All Pure proposes to analyze the soils samples for volatile organic compounds (VOCs), but does <br /> not state the analytical method to be used. The toxicity characteristic leaching procedure <br /> (TCLP) should be used on the soil samples to be analyzed for VOCs. This method uses a zero <br /> headspace extractor to allow accurate assessment of leachable VOCs in a waste. The TCLP <br /> extraction solution should be deionized water. The analytical method used should be able to <br /> achieve detection limits no greater than the water quality limits listed in the attached Volatile <br /> Organic Contaminants Found in Ground Water at Class III Landfills. <br /> The analyses requested for general minerals, pH, electrical conductivity (EC), and total <br /> dissolved solids (TDS) are necessary since nitrates, chloride, EC, and TDS are known to be <br /> elevated in the ground water in the area of the ponds. It is necessary to determine the potential <br /> of the soils to further impact ground water quality with regard to these parameters. The TCLP <br /> with deionized water should also be used on soil samples to be analyzed for these parameters. <br /> The standard protocols for analysis of water for these parameters should be conducted on the <br /> extract from the TCLP. <br /> All Pure should propose the analytical methods to be used on the extract from the TCLP for <br /> VOCs, general minerals, pH, EC, and TDS. Detection limits for VOCs should be stated. <br /> Task 5 - Report <br /> All Pure proposes to submit a report describing the sampling procedures and analytical results <br /> following receipt of the analytical results. The report is proposed to include a description of the <br /> methods and construction schedule to achieve closure of the surface impoundments. Closure is <br /> proposed to be accomplished by backfilling with clean compacted native soil and grading to <br /> prevent ponding of surface water over the closed impoundments and divert runoff to the south. <br /> The report on soil sampling should include the proposed disposal method and/or remediation <br /> method for all contaminated soils and the source of soil to be used as backfill. Laboratory <br /> analyses may be required for the fill soils before backfilling. The report should also include <br /> cleanup levels to be achieved in the ponds, an estimate of volume of soils to be excavated, <br /> removed, or remediated, a grading plan, and proposals for confirmation sampling and soil <br /> compaction. Chapter 15 requirements for closure of the surface impoundments will not apply if <br /> no contaminants remain in the soil. The schedule to be included in the report must include <br /> schedules for submittal of a closure report and construction of any building over the <br /> impoundment areas. <br /> The closure report must report the date of closure of each pond, the volume of soil excavated, <br /> removed, or remediated, all analytical results for soils removed or remediated and all <br /> confirmation samples, percent compaction of the soils, and the final grading plot. Closure of the <br /> impoundments must be under the direct supervision of a registered civil engineer or certified <br /> engineering geologist. The responsible engineer or geologist must sign the report and include <br /> his or her stamp with expiration date if an engineer, or registration number if a geologist. <br />