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MAR 12 92 14:45 C.KC: 9163715821 � P. 1 <br /> 4. Each sample will be received by the,laboratory within two days of collection. <br /> Samples will be kept in a clean ice-cooled chest. "Blue Ice" is recommended instead <br /> of ice during transport to the laboratory. All samples will be delivered to the <br /> laboratory under chain-of-custody documentation., with the original included in the ice <br /> chest. A copy of the chain-of-custody will be kept for the project file. <br /> 5. finless otherwise requested by the laboratory, no preservatives will be added to the <br /> sample. <br /> 6. The sealed sample container will be opened only by the laboratory personnel who will <br /> perform the chemical analysis. The samples will be analyzed within 7 to 14 days <br /> from their collection date depending can EPA quality control criteria appropriate for <br /> each analytical method. <br /> 7. ,lie analytical laboratory will provide laboratory quality assurancelquality control <br /> documentation. This will include results from method spike, method blank analyses, <br /> and duplicate analysis tone duplicate for every ten samples analyzed). <br /> Sample Collection <br /> i. Groundwater samples will not be collected until the well � been allowed to stabilize <br /> for 24 fours following well development. Prior to purging, the water level in the <br /> well will be measured and the well checked for free floating product. The water level <br /> in the well will be checked with an electronic well sounder. The well will be checked <br /> for free floating product by utidzing a transparent bailer to collect a liquid sample <br /> from the water surface. The liquid sample inside the bailer will then be visually <br /> examined for evidence of free floating product. The thickness of any free floating <br /> R, product layer will be recorded in the field notes. Water samples will also be inspected <br /> for the presence of odor and/or sheen. <br /> a <br /> Each well will be purged of water prior to the collection of the water sample. Three <br /> to five well volumes will be removed from the well by bailing or pumping. After <br /> three to five well volumes have been removed from the well, three successive water <br /> samples will be measured for pH, conductivity, and temperature using properly <br /> calibrated instrumentation. Well purging shall continue until the measurements from <br /> three successive water samples are constant. <br /> 3. All well purge water will be recovered and placed in 55-gallon drums. The well will <br /> be .allowed to recover to at least 80 percent of originally measured water level before <br /> a water sample is collected. <br /> 4. Equipment used for well purging will be thoroughly steam-cleaned or cleaned in soapy <br /> (TSP) water, rinsed with clean tap water, and finally rinsed with de-ionized water <br /> prior to the use in each well. <br /> .46 A-4 <br />