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Alpha Analytical, Inc. <br /> 255 Glendale Ave. •Suite 21 •Sparks,Nevada 89431-5778 <br /> (775)355-1044•(775)355-0406 FAX• 1-800-283-1183 <br /> Date: Work Order: <br /> 24-May-13 QC Summa Report 13051542 <br /> Method Blank Type:MBLK Test Code:EPA Method SW8015B/C Ext <br /> File ID:1A05211305.D Batch ID:30966 Analysis Date: 05/21/201312:04 <br /> Sample ID: MBLK-30966 Units:mg/Kg Run ID:FID_1_130520A Prep Date: 05/20/2013 11:00 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPDRefVal %RPD(Limit) Qual <br /> TPH-E(DRO) ND 5 <br /> TPH-E(ORO) ND 10 <br /> Surr:Nonane 7.24 6 121 65 160 <br /> Laboratory Control Spike Type:LCS Test Code:EPA Method SW8015B/C Ext <br /> File ID:1A05211306.11) Batch ID:30966 Analysis Date: 05/21/2013 12:29 <br /> Sample ID: LCS-30966 Units:mg/Kg Run ID:FID_1_130520A Prep Date: 05120/201311:00 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPDRefVal %RPD(Limit) Qual <br /> TPH-E(DRO) 98.4 5 100 98 70 130 <br /> Surr:Nonane 7.47 6 124 65 160 <br /> Sample Matrix Spike Type:MS Test Code:EPA Method SW8015B/C Ext <br /> File ID:1A05211330.D Batch ID:30966 Analysis Date: 05/21/2013 22:35 <br /> Sample ID: 13051722-06AMS Units:mg/Kg Run ID:FID 1_130520A Prep Date: 05/20/201311:00 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPDRefVal %RPD(Limit) Qual <br /> TPH-E(DRO) 7260 50 100 5465 1800 46 150 M3 <br /> Surr:Nonane 0 6 0 65 160 S50 <br /> Sample Matrix Spike Duplicate Type:MSD Test Code:EPA Method SW8015B/C Ext <br /> File ID:1A05211331.11) Batch ID:30966 Analysis Date: 05/21/2013 23:00 <br /> Sample ID: 13051722-06AMSD Units:mg/Kg Run ID:FID_1_130520A Prep Date: 05/20/201311:00 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPDRefVal %RPD(Limit) Qual <br /> TPH-E(DRO) 7260 50 100 5465 1800 46 150 7264 0.0(42) M3 <br /> Surr:Nonane 0 6 0 65 160 S50 <br /> Comments: <br /> Calculations are based off of raw(non-rounded)data.However,for reporting purposes,all QC data is rounded to three significant figures.Therefore,hand calculated <br /> values may differ slightly. <br /> M3=The accuracy of the spike recovery value is reduced since the analyte concentration in the sample is disproportionate to the spike level.The method control <br /> sample recovery was acceptable. <br /> S50=The analysis of the sample required a dilution such that the surrogate concentration was diluted below the laboratory acceptance criteria.The laboratory control <br /> sample recovery was acceptable. <br />