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Alpha Analytical, Inc. <br /> 255 Glendale Ave. •Suite 21 •Sparks,Nevada 89431-5778 <br /> (775)355-1044•(775)355-0406 FAX• 1-800-283-1183 <br /> Date: (� 111I11a Report Work Order: <br /> 28-May-13 QC Summary <br /> p 13051542 <br /> Method Blank Type:MBLK Test Code:EPA Method SW8260B <br /> File ID:13052006.D Batch ID:MS08SO953A Analysis Date: 05/20/2013 13:49 <br /> Sample ID: MBLK MS08SO953A Units:pg/Kg Run ID:MSD_08_130520A Prep Date: 05/20/201313:49 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPDRefVal %RPD(Limit) Qual <br /> Chloromethane ND 40 <br /> Vinyl chloride ND 20 <br /> Chloroethane ND 20 <br /> Bromomethane ND 40 <br /> Trichlorofluoromethane ND 20 <br /> 1,1-Dichloroethene ND 20 <br /> Dichloromethane ND 40 <br /> trans-1,2-Dichloroethene ND 20 <br /> 1,1-Dichloroethane ND 20 <br /> cis-1,2-Dichloroethene ND 20 <br /> Chloroform ND 20 <br /> 1,2-Dichloroethane ND 20 <br /> 1,1,1-Trichloroethane ND 20 <br /> Carbon tetrachloride ND 20 <br /> Benzene ND 5 <br /> 1,2-Dichloropropane ND 20 <br /> Trichloroethene ND 20 <br /> Brom od ich lorom ethane ND 20 <br /> cis-1,3-Dichloropropene ND 20 <br /> trans-1,3-Dichloropropene ND 20 <br /> 1,1,2-Trichloroethane ND 20 <br /> Toluene ND 5 <br /> Dibromochlorom ethane ND 20 <br /> Tetrachloroethene ND 20 <br /> Chlorobenzene ND 20 <br /> Ethylbenzene ND 5 <br /> m,p-Xylene ND 5 <br /> Bromoform ND 20 <br /> o-Xylene ND 5 <br /> 1,1,2,2-Tetrachloroethane ND 20 <br /> 1,3-Dichlorobenzene ND 20 <br /> 1,4-Dichlorobenzene ND 20 <br /> 1,2-Dichlorobenzene ND 20 <br /> Surr: 1,2-Dichloroethane-d4 222 200 111 70 130 <br /> Surr:Toluene-d8 204 200 102 70 130 <br /> Surr:4-Bromofluorobenzene 191 200 95 70 130 <br /> Laboratory Control Spike Type:LCS Test Code:EPA Method SW8260B <br /> File ID:13052027.D Batch ID:MS08SO953A Analysis Date: 05/20/2013 22:18 <br /> Sample ID: LCS MS08SO953A Units:pg/Kg Run ID:MSD 08 130520A Prep Date: 05/20/2013 22:18 <br /> D <br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPDRefVal %RPD(Limit) Qual <br /> 1,1-Dichloroethene 163 20 400 41 10 131 <br /> Benzene 426 10 400 107 70 137 <br /> Trichloroethene 441 20 400 110 70 149 <br /> Toluene 409 10 400 102 70 139 <br /> Chlorobenzene 396 20 400 99 70 137 <br /> Ethylbenzene 433 10 400 108 70 137 <br /> m,p-Xylene 414 10 400 104 70 145 <br /> o-Xylene 418 10 400 105 70 145 <br /> Surr. 1,2-Dichloroethane-d4 432 400 108 70 130 <br /> Surr:Toluene-d8 393 400 98 70 130 <br /> Surr:4-Bromofluorobenzene 424 400 106 70 130 <br />