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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC. Telephone: 925-798-1620 Fax : 925-798-1622 <br /> http://www.mcratnpbcli.com E-mail:main@mccampbell.com <br /> Advanced GeoEnvironmental Client Project ID: Spingolo Trucking Date Sampled: 10/04/01 <br /> 837 Shaw Road Date Received: 10/05/01 <br /> iStockton, CA 95215 Client Contact:Paul Dotson. Date Extracted: 10/05/01 <br /> Client P.O: Date Analyzed: 10/05-10/08/01 <br /> Diesel Range(C10-C23) and Oil-Range(C18+)Extractable Hydrocarbons as Diesel and Motor Oil* <br /> EPA methods modified 8015,and 3550 or 3510;California RWQCB(SF Bay Region)method GCFID(3550)or GCFID(3510) <br /> Lab ID Client ID Matrix TPH(d)+ TPH(mo)+ %Recovery <br /> Surrogate <br /> 80236 P1-25 S 4700,a 1400 98 <br />' 80239 Pi-40 S 1800,a 570 99 <br /> 80240 PI-45 S 3700,a 1200 97 <br /> 80243 P2-20 S ND ND 99 <br /> 80245 P2-30 S 9.1,a ND 99 <br /> lie <br /> I <br /> i <br /> I <br /> Reporting Limit unless otherwise W 50 ug(L 250 ug/L <br /> I stated;ND means not detected above <br /> the reporting limit S 1.0 mg/kg 5.0 mg/kg <br /> *water samples are reported in ug/L,wipe samples in ug/wipe,soil and sludge samples in mg/kg,and all TCLP/STLC/SPLP extracts in <br /> I <br /> ug/L <br /> "cluttered chromatogram resulting in coeluted surrogate and sample peaks,or;surrogate peak is on elevated baseline,or;surrogate has been <br /> diminished by dilution of original extract. <br /> I 'The fallowing descriptions of the TPH chromatogram are cursory in nature and McCampbel] Analytical is not responsible for their <br /> interpretation:a)unmodified or weakly modified diesel is significant;b)diesel range compounds are significant;no recognizable pattern;c) <br /> aged diesel?is significant);d)gasoline range compounds are significant;e)medium boiling point pattern that does not match diesel(?); f) <br /> one to a few isolated peaks present; g) oil range compounds are significant; h) lighter than water immiscible sheen is present; i) liquid <br /> Isample that contains greater than—5 vol.%sediment. <br /> DHS Certification No. 1644 ��Edward Hamilton,Lab Director <br /> I <br />