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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL. INC. Telephone: 925-798-1620 Fax: 925-798-1622 <br /> httpa/www_mc_campbell.com E-mail:main@mccampbell.com <br /> Advanced GeoEnvironmental Client Project ID: Spingolo Trucking Date Sampled: 10/04/01 <br /> 837 Shaw Road Date Received: 10/05/01 <br /> Stockton, CA 95215 Client Contact: Paul Dotson Date Extracted: 10/05/01 <br /> Client P.O: Date Analyzed: 10/11/01 <br /> Seven Oxygenated Volatile Organics By /MS <br /> EPA method 8260 modified GC <br /> Lab ID 80236 80239 80240 80243 <br /> Reporting Limit <br /> Client[D P1-25 P140 P145 P2-20 <br /> Matrix S S S S S W <br /> Compound Concentration* ug/kg ug/L <br /> IDi-isopropyl Ether(DIPE) ND ND ND ND 5.0 1.0 <br />' Ethyl tert-Butyl Ether(ETRE) ND ND ND ND 5.0 1.0 <br /> . Methyl tert-Butyl Ether(MTBE) ND ND ND ND 5.0 1.0 <br /> tert-Amyl Methyl Ether(TAME) ND ND ND ND 5.0 1.0 <br />' tert-Butanol ND ND ND ND 25 5.0 <br /> Methanol ND ND ND ND 2500 500 <br /> Ethanol ND ND ND ND 250 50 <br /> -I L <br /> Surrogate Recoveries(%) <br /> Dibromotluoromethane 100 E <br /> 99 99 <br /> Comments: <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br />' ND means not detected above the reporting limit;NIA means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than—5 vol.%sediment;(j)sample diluted due to <br /> high organic content <br /> I <br /> DHS Certification No. 1644 �dward Hamilton,Lab Director <br /> I <br />