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n <br /> McCam bell Analytical, Inc. 1534 Willow Pass Road,Pittsburg,CA 94565-1701 <br /> Web:%wwmccampbellxom E-mail:mnin@mccarnpbcll.coni <br /> "When Quality Counts" Telc have:877-252-9262 rax:925-252-9269 <br /> QC SUMMARY REPORT FOR SM5520E/F <br /> W.O.Sample Matrix: Soil OC Matrix. Soil WorkOrder 0807078 <br /> EPA Method SM5520EIF Extraction SM5520EIF BatchlD: 36611 Spiked Sample ID: 0806812-001A <br /> Analyte Sample SpikedE%Rec. <br /> MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria(%) <br /> mglKg mg/Kg %Rec. %RPI) %Rec. %Rec. %RPD MS I MSD RPD LCSILCSD RPD <br /> POC 690 I000 111 1 2.24 106 103 3.37 70- 130 30 70- 130 30 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: <br /> NONE <br /> BATCH 36611 SUMMARY <br /> Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Dale Extracted Date Analyzed <br /> 0807078-001A 06130108 11:00 AM 07/02/08 07/07/08 2:21 PM 0807078-002A 06/30/08 11:00 AM 07/02/08 07/07/08 2:26 PM <br /> 0807078-003A 06130/08-11:00 AM 07/02/08 07/07/08 2:31 PM 0807078-004A 06/30/08 11:00 AM 07/02/08 07/07/08 2:36 PM <br /> 0807078-005A 06/30/08 11:00 AM 07/02/08 07/07/08 2:41 PM 0807078.006A 06/30/06 11:00 AM 07/02/08 07/07/08 2:46 PM <br /> MS=Matrix Spike:MSD=Matrix Spike Duplfcote;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate;RPD=Relative Percent Deviation. <br /> %Recovery=100.(MS Sample)I(Amount Spiked);RPD=1 nn'(MS- MSD)/((MS t MSD)12). <br /> MS I MSD spike recoveries and 1 or%RPD may fall outside of laboratory acceptance criteria due to one or more of the follawirig reasons:a)the sample is inhomogenous AND <br /> contains signitirmnt concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. <br /> NIA=not enough sample to perform matrix sp#ice and matrix spike dupfieate. <br /> NR=analyte concentration In sample exceeds spike amount for soil matrix or exceeds Dr spike amount for water matrix or sample diluted due to high matrix or analyte content <br /> D1-1S FLAP Certification 1644 J2— QAIQC Officer <br /> I <br /> I <br />