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. I <br /> [ 1 <br /> � !cal, SDC. <br /> �,& I534tvillowPusRoatl,Pittsburg,CA 94565-1701 <br /> McCampbell Anal <br /> CdyLWeb:www.moaimpbell.mm C-mail:muin@m=mpbLIt.com <br /> l"f�G <br /> "Mum OualitvCounts" Te10 bone:877-2752.9261 fnx:925-252-9269 <br /> QC SUMMARY REPORT FOR SW8015C <br /> W.O.Sample Matrix: Soil QC Matrix: Sal WorkOrder 0807078 <br /> EPA Method SW8015C Extraction SW3550C SatchlD: 36685 Spiked Sample ID: 0607046-002A <br /> Analyte Sample Spiked MS MSD MS_MSD ' LCS LCSD LCS-LCSD Acceptance Criteria(%) <br /> mg/Kg mglKg %Rec. %Rec. %RPD %Rec_ %Rec. %RPD MS 1 MSD RPD LCS/LCSD I RPD <br /> TPN-Diesel(CIO-C23) 4.0 20 98.4 96.9 1.24 t00 102 1.55 70- 130 30 70- 130 30 <br /> 107 50 117 118 0.336 109 100 8.31 70-I30 30 70- 130 30 <br /> All target compounds in the Method Blank of this extraction hatch were ND less than the method RL with the following exceptions: <br /> NONE <br /> BATCH 36685 SUMMARY <br /> Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date Extracted Date Analyzed <br /> 0807078-OOIA 06/30/08 11:00 AM 07/02/08 07/07/08 10:26 AM 0807078-002A 06/30/08 11:00 AM 07/02/08 07/03/08 6:47 PM <br /> 0807078-003A 06/30/08 11:00 AM 07/02/08 07/03/08 5:38 PM 0807078-004A 06/30/08 11:00 AM. 07/02/08 07/04/08 12:29 AM <br /> 0807078-005A 06/30108 11:00 AM 07/02/08 07/03/08 10:12 PM GR07078-006A 06/30/08 11:00 AM 07/02/08 07/03/08 9:03 PM <br /> i <br /> MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate;RPD=Relative Percent Deviation. <br /> %Recovery=100'(MS-Sample)I(Amount Spkedl;RPO=100'(IVIS- MSD)I((MS+MSD)12), <br /> MS 1 MSD spike recoveries and 1 or%R PO may fall outside of laboratory acceptance criteria due to one or more of the following reasons:a)the sample is inhomagenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix Interferes with the spike recovery. <br /> NIA=not enough sample to perform matrix spike and matrix spike duplicate. <br /> NR=analyte concentration In sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. <br /> Dl-1S FLAP Certification 1644 J2_ QA/QC Officer <br />