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Castle Analytical Laboratory, Atwater, CA <br /> Lab Report No.: H4061408 Date: 06/25/2004 Page: 12 <br /> Project Name: OLIVAREZ PROPERTY Analysis: Volatile Organic Compounds by GC/MS Fuel <br /> Project No: NA Method: 8260FA <br /> Prep Meth: SW50308 <br /> Field ID: MW-9 Lab Samp ID: 7059-11W <br /> Descr/Location: MW-9 Recd Date: 06/15/2004 <br /> Sample Date: 06/11/2004 Prep Date' 06/23/2004 <br /> Sample Time: 1600 Analysis Date: 06/23/2004 <br /> Matrix: Water QC Batch: VWMS-6234 <br /> Basis: Not Filtered Notes: <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tent-butyl ether(MTBE) 0.289 0.5 MRL NO UG/L 1 <br /> Ethyl tert-butyl ether(ETBE) 0.084 0.5 MRL NO UG/L 1 <br /> tert-Amyl methyl ether(TAME) 0.067 0.5 MRL NO UG/L 1 <br /> Di-isopropyl ether(DIPE) 0.155 0.5 MRL NO UG/L 1 <br /> tent-Butyl alcohol (TBA) 8.79 20. MRL NO UG/L 1 <br /> 1,2-Dichloroethane 0.081 0.5 MRL NO UG/L 1 <br /> 1,2-Dibromoethane 1 0.092 0.5 MRL NO UG/L 1 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> Toluene-d8 63-132 SLSA 102% 1 <br /> 1,2-Dichloroethane-d4 59-135 SLSA 99.0% 1 <br /> Approved by: Date: <br />