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Castle Analytical Laboratory, Atwater, CA <br /> kl <br /> Lab Report No.: H4061408 Date: 06/25/2004 Page: 1 <br /> Project Name: OLIVAREZ PROPERTY Analysis: Volatile Organic Compounds by GC/MS Fuel <br /> Project No: NA Method: 8260FA <br /> Prep Meth: SW50308 <br /> Field ID: EW-1 Lab Samp ID: 7059-12W <br /> Descr/Location: EW-1 Recd Date: 06/15/2004 <br /> Sample Date: 06/11/2004 Prep Date: 06/23/2004 <br /> Sample Time: 1628 Analysis Date: 06/23/2004 <br /> Matrix: Water QC Batch: VWMS-6234 <br /> Basis: Not Filtered Notes: DF <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 28.9 50. MRL 750. UG/L 100 <br /> Ethyl tert-butyl ether(ETBE) 8.40 50, MRL ND UG/L 100 <br /> tert-Amyl methyl ether(TAME) 6.70 50. MRL ND UG/L 100 <br /> Di-isopropyl ether(DIPE) 15.5 50, MRL ND UG/L 100 <br /> tert-Butyl alcohol (TBA) 879. 2000. MRL ND UG/L 100 <br /> 1,2-Dichloroethane 8.10 50. MRL 38Q UG/L 100 <br /> 1,2-Dibromoethane 1 9.20 50. MRL 300. UG/L 100 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> Toluene-d8 63-132 SLSA 99.7% 1 <br /> 1,2-Dichloroethane-d4 59-135 SLSA 87.2% 1 <br /> DF: Reporting limits elevated due to matrix interferences <br /> Approved by: Date: <br />