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Castle Analytical Laboratory, Atwater, CA <br /> ~ Lab Report No.: H4032502 Date: 04/02/2004 Page: 4 <br /> =No: <br /> ILIVAREZ PROPERTY Analysis: Volatile Organic Compounds by GC/MS Fuel <br /> A Method: 8260FA <br /> Prep Meth: SW5030B <br /> Field ID: R M IM-Z �"� Lab Samp ID: 6797-3W <br /> Descr/Location: U%N4R M IN -a r+ Recd Date: 03/25/2004 <br /> Sample Date: 03/23/2004 Prep Date: 03/31/2004 <br /> Sample Time: 1300 Analysis Date: 03/31/2004 <br /> Matrix: Water OC Batch: VWMS-3314 <br /> Basis: Not Filtered Notes: OF <br /> Analyte Dei Limit Rep Limit Note Result Units Pvc Oil <br /> Methyl-tert-butyl ether(MTBE) 2.89 5. MRL 12Q UG/L 10 <br /> Ethyl tert-butyl ether(ETBE) 0.840 5. MRL NO UG/L 10 <br /> tert-Amyl methyl ether(TAME) 0.670 5. MRL NO UG/L 10 <br /> Di-isopropyl ether(RIPE) 1.55 5. MRL NO UGIL 10 <br /> tert-Butyl alcohol (TBA) 87.9 200. MRL NO UG/L 10 <br /> 1,2-Dichloroethane 0.810 5. MRL 15Q UGIL 10 <br /> 1,2-Dibromoethane 0.920 5. MRL 14, UG/L 10 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> Toluene-d8 76.129 SLSA 100% 1 <br /> 1,2-Dirhloroethane-d4 53-141 SLSA 94.5% 1 <br /> DF: Reporting limits elevated due to matrix interferences <br /> Approved by:__6AZ Date: <br />