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Castle Analytical Laboratory, Atwater, CA <br /> Lab Report No.: H4032502 Date: 04/02/2004 Page: 5 <br /> Project Name: OILIVAREZ PROPERTY Analysis: Volatile Organic Compounds by GC/MS Fuel <br /> Project No: NA Method: • 8260FA <br /> Prep Meth: SW5030B <br /> Field ID: MW-3 Lab Samp ID: 6797-4W <br /> Descr/Location: MW-3 Recd Date: 03/25/2004 <br /> Sample Date: 03/23/2004 Prep Date: 03/31/2004 <br /> Sample Time: 0902 Analysis Date: 03/31/2004 <br /> Matrix: Water QC Batch: VWMS-3314 <br /> Basis: Not Filtered Notes: <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Oil <br /> Methyl-ter#-butyl ether(MTBE) 0.289 0.5 MRL NO UG/L 1 <br /> Ethyl tert-butyl ether(ETBE) 0.084 0.5 MRL ND UGIL 1 <br /> tert-Amyl methyl ether(TAME) 0.067 0.5 MRL NO UG/L 1 <br /> Di-isopropyl ether(DIPE) 0.155 0.5 MRL NO UG/L 1 <br /> tent-Butyl alcohol (TBA) 8.79 20. MRL NO UG/L 1 <br /> 1,2-Dichloroethane 0.081 0.5 MRL 32 UG/L 1 <br /> 1,2-Dibromoethans 0.092 0.5 MRL NO UGIL 1 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> Toluene-d8 76-129 SLSA 101% 1 <br /> 1,2-Dichloroethane-d4 53-141 SLSA 99.5% 1 <br /> Date: <br /> Approved by: y� n <br />